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Method for manufacturing polyurethane microporous automotive buffer block

A manufacturing method and buffer block technology are applied in the manufacturing field of polyurethane microporous automobile buffer blocks, which can solve the problems of high dynamic fatigue deformation rate, affecting the service life of products, poor comprehensive mechanical properties, etc., so as to improve dynamic fatigue resistance performance, improve The effect of elasticity, improved dynamic fatigue resistance and comprehensive mechanical properties

Active Publication Date: 2011-11-30
江苏邦博聚氨酯新材料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] In the above-mentioned preparation method, the dynamic fatigue deformation rate of the product is high, and the comprehensive mechanical properties are poor. These shortcomings affect the service life of the product, especially when it is used as a damping element in the field of automobiles, these indicators are particularly important.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0019] Add 500 g of polytetrahydrofuran polyols by parts 3000 in a 2 liter reactor, add 25 g of glass micropowder after processing, 2 g of n-butyl titanate, 40 g of sodium dimethyl sulfonate isophthalate, and raise the temperature of the material to 80° C., under the protection of nitrogen, an excess of 4,4-diphenylmethane diisocyanate was added, and the temperature was maintained for 2 hours to obtain a prepolymer with an —NCO content of 7.2%.

[0020] The auxiliary agent in the chain extender component accounts for 10% of the total amount of the chain extender, and the ratio of the prepolymer to the chain extender component is 100:8.8. Use a low-pressure foaming machine to inject the mixture of prepolymer and chain extender components into a mold at 90°C, pre-cure in an oven at 90°C for 5 hours, demould, and then put it in an oven at 100°C for 15 hours to obtain products.

Embodiment 2

[0022] Add 500 g of polytetrahydrofuran polyols by parts 4000 in a 2-liter reactor, add 15 g of treated glass micropowder, 2 g of n-butyl titanate, and 40 g of sodium dimethyl sulfonate isophthalate. to 90° C., under the protection of nitrogen, an excess of 4,4-diphenylmethane diisocyanate was added, and the temperature was maintained for 4 hours to obtain a prepolymer with an —NCO content of 7.2%.

[0023] The auxiliary agent in the chain extender component accounts for 10% of the total amount of the chain extender, and the ratio of the prepolymer to the chain extender component is 100:10. Use a low-pressure foaming machine to inject the mixture of prepolymer and chain extender components into a mold at 90°C, pre-cure in an oven at 90°C for 3 hours, then release the mold, and then put it in an oven at 100°C for 12 hours to obtain products.

Embodiment 3

[0025] Add 500 g of polytetrahydrofuran polyols by parts 6000 in a 2-liter reactor, add 20 g of treated glass micropowder, 2 g of n-butyl titanate, and 45 g of sodium dimethyl sulfonate isophthalate. To 85° C., under the protection of nitrogen, an excess of 4,4-diphenylmethane diisocyanate was added, and the temperature was maintained for 3 hours to obtain a prepolymer with an -NCO content of 7.2%.

[0026] The auxiliary agent in the chain extender component accounts for 10% of the total amount of the chain extender, and the ratio of the prepolymer to the chain extender component is 100:12. Use a low-pressure foaming machine to inject the mixture of prepolymer and chain extender components into a mold at 90°C, pre-cure in an oven at 90°C for 5 hours, then release the mold, and then put it in an oven at 110°C for 15 hours to obtain products.

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PUM

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Abstract

The invention discloses a method for manufacturing a polyurethane microporous automotive buffer block, aiming at overcoming the defects of the prior art and improving the dynamic fatigue deformation rate and the comprehensive mechanical properties of the polyurethane microporous automotive buffer block. The method for manufacturing the polyurethane microporous automotive buffer block has the advantages of improving the dynamic fatigue deformation rate and the comprehensive mechanical properties of the polyurethane microporous automotive buffer block by adopting the novel polyether glycol with low unsaturation degree and high molecular weight (3000-6000) and inducing 3-5 percent nano-glass micro powder into the novel polyether glycol, i.e. the method improves the elasticity and the dynamic fatigue deformation rate of the polyurethane microporous automotive buffer block by adopting the polyether glycol with low unsaturation degree and high molecular weight, and improves the comprehensive mechanical properties of the polyurethane microporous automotive buffer block such as the intensity and the like by inducing the nano-glass micro powder, thereby solving the problem that the polyurethane foam elastomer has poor comprehensive mechanical properties and dynamic fatigue deformation rate.

Description

technical field [0001] The invention relates to a method for preparing a novel polyurethane foamed elastomer, in particular to a method for manufacturing a polyurethane microporous automobile buffer block. Background technique [0002] Because polyurethane microcellular elastomer has excellent dynamic and static mechanical properties, it is especially suitable for anti-seismic and damping systems, and most of them are used in stop buffer blocks in the automotive industry. However, the current domestic production of polyurethane foam elastomers is as follows: first, the molecular weight is 1000-3000 polyester (or polyether) polyol and 4,4-diphenylmethane diisocyanate (hereinafter also referred to as: MDI) in At 70-90°C, a prepolymer with an isocyanate group (hereinafter also referred to as: -NCO) content of about 10% is formed, which is composed of a chain extender, a foaming agent, a foam stabilizer, a foam stabilizer, and a catalyst. agent, mix the prepolymer and the addit...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08L75/08C08K13/02C08K3/40C08K5/42C08G18/48C08J9/12C08G101/00
Inventor 孙俭
Owner 江苏邦博聚氨酯新材料有限公司