Method for preparing molecular imprinted polymer on surface of carbon microspheres

A technology of surface molecular imprinting and carbon microspheres, which is applied in the field of preparation of molecularly imprinted polymers on the surface of carbon microspheres, and can solve the problems such as the difficulty of combining the molecules to be recognized and the recognition sites.

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  • Abstract
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  • Application Information

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Problems solved by technology

[0003] The matrix of molecularly imprinted materials can be inorganic materials, such as silica gel, alumina, etc., or polymer materials, but most of the recognition sites of polymer microspheres are inside the polymer microspheres. When recognizing larger molecules, the diffusion resistance The presence of will make it difficult for the molecule to be recognized to bind to the recognition site

Method used

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  • Method for preparing molecular imprinted polymer on surface of carbon microspheres
  • Method for preparing molecular imprinted polymer on surface of carbon microspheres
  • Method for preparing molecular imprinted polymer on surface of carbon microspheres

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Embodiment Construction

[0181] The present invention will be further described below in conjunction with accompanying drawing:

[0182] figure 1 As shown, the state diagram of carbon microspheres is prepared, and the position and connection relationship of each part must be correct.

[0183] Acetylene gas is the raw material for preparing carbon microspheres, and argon gas is the carrier gas and protective gas, which can also drive out harmful substances in the quartz tube, and the gas flow rate must be strictly controlled.

[0184] The high temperature section in the quartz tube is the gas phase generation section of the carbon microsphere product.

[0185] figure 2 As shown, the state diagram is prepared for imprinted carbon microspheres, and the position and connection relationship of each part must be correct.

[0186] The oxidation, modification, and imprinting of imprinted carbon microspheres in the preparation process are all completed in a three-necked flask. They are all completed in seq...

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Abstract

The invention relates to a method for preparing a molecular imprinted polymer on the surface of carbon microspheres, which comprises the following steps of: preparing the carbon microspheres by using acetylene gas; and preparing imprinted carbon microspheres on a three-neck flask, a water bath and an electrothermal stirring vessel, namely performing oxidation treatment on the carbon microspheres and then performing surface modification on the oxidized carbon microspheres to prepare the imprinted carbon microspheres and form irregular hole prints on the surface of the carbon microspheres. The preparation method has the advantages of advanced and reasonable process, short process flow, less environmental pollution, attractive appearance of a product, high purity of 99 percent and high product yield of 91 percent; the imprinted carbon microspheres are black and round particles with the particle diameter of 100 to 200nm and can be matched with various chemical substances; the method is an ideal method for preparing the imprinted carbon microspheres; and the product can be applied to the fields of pharmacy and various industries.

Description

technical field [0001] The invention relates to a method for preparing molecularly imprinted polymers on the surface of carbon microspheres, which belongs to the technical field of organic carbon material-carbon microsphere surface functional modification and application. Background technique [0002] Molecular imprinting technology is an emerging subject, which is to imprint template molecules on a certain substrate, so that the substrate has specific selectivity and binding ability for template molecules, so that it can be used for the separation, enrichment and detection of template molecules. It shows good application prospects in the fields of chiral separation, solid phase extraction, enrichment, detection, enzyme simulation, and chemical bionic sensors. [0003] The matrix of molecularly imprinted materials can be inorganic materials, such as silica gel, alumina, etc., or polymer materials, but most of the recognition sites of polymer microspheres are inside the polym...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08F292/00C08F2/44C08F220/06C08K5/45C08J9/26C01B31/02B01J20/30B01J20/26B01J20/28
Inventor 刘旭光杨永珍郭明聪李莎刘伟峰许并社
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