Method for preparing animal semen freeze-dried powder
A technology of freeze-dried powder and semen, which is applied in the direction of freeze-dried transportation, medical raw materials derived from mammals, powder transportation, etc., which can solve the problems of microorganisms losing biological vitality, texture hardening, loss, etc., and achieve the effect of high medicinal value
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Embodiment 1
[0032] A method for preparing animal semen freeze-dried powder, which is prepared by freeze-drying fresh semen, including the steps of pre-freezing, sublimation drying and analysis drying. The specific operation steps are as follows:
[0033] (1) Aseptically collect fresh donkey semen to remove flocculent turbidity and put it into a material tray, the thickness of the semen is 3.0mm;
[0034] (2) Put the above-mentioned material tray with semen into the clapboard of the cold hydrazine of the vacuum freeze dryer, the temperature of the cold hydrazine of the vacuum freeze dryer drops to -40°C, the temperature of the divider drops to -30°C, and the temperature of the material material is at -40°C. Pre-freeze at -26°C for 6 hours;
[0035] (3) Take out the cold hydrazine from the material tray, turn on the vacuum pump, and sublimate and dry at a vacuum degree of 1.5 Pa. The temperature of the partition is 0° C., and the temperature of the material is -38° C. for 3 hours;
[0036]...
Embodiment 2
[0048] A method for preparing animal semen freeze-dried powder, which is prepared by freeze-drying fresh semen, including the steps of pre-freezing, sublimation drying and analysis drying. The specific operation steps are as follows:
[0049] (1) Aseptically collect fresh donkey semen to remove flocculent turbidity and put it into a material tray, the thickness of the semen is 4.0mm;
[0050] (2) Put the above-mentioned material tray with semen into the clapboard of the cold hydrazine of the vacuum freeze dryer, the temperature of the cold hydrazine of the vacuum freeze dryer drops to -50°C, the temperature of the clapboard drops to -40°C, and the temperature of the material material is at -50°C. Pre-freeze at -39°C for 5 hours;
[0051] (3) Take out the cold hydrazine from the material tray, turn on the vacuum pump, and sublimate and dry at a vacuum degree of 5 Pa. The temperature of the partition is 1° C., and the temperature of the material is -34° C. for 2 hours;
[0052]...
Embodiment 3
[0055] A method for preparing animal semen freeze-dried powder, which is prepared by freeze-drying fresh semen, including the steps of pre-freezing, sublimation drying and analysis drying. The specific operation steps are as follows:
[0056] (1) Aseptically collect fresh donkey semen to remove flocculent turbidity and put it into a material tray, the thickness of the semen is 5.0mm;
[0057] (2) Put the above-mentioned material tray with semen into the clapboard of the cold hydrazine of the vacuum freeze dryer, the temperature of the cold hydrazine of the vacuum freeze dryer drops to -45°C, the temperature of the clapboard drops to -46°C, and the temperature of the material material is at -45°C. Pre-freeze at -45°C for 4 hours;
[0058] (3) Take out the cold hydrazine from the material tray, turn on the vacuum pump, and sublimate and dry at a vacuum degree of 10 Pa. The temperature of the separator is 2° C., and the temperature of the material is -31° C. for 2 hours;
[0059...
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