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Method for comprehensively utilizing and processing gracilaria

A processing method and technology of Gracilaria, applied in the field of comprehensive utilization of Gracilaria, can solve problems such as polluting the environment and wasting resources

Inactive Publication Date: 2013-03-20
FISHERIES RES INST OF FUJIAN
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0016] The purpose of the present invention is to only extract the agar in the algae for the existing method for extracting the glue from Gracilaria, and the phycoerythrin and the cellulose in the algae are all discharged into the sea as sewage and rubbish or transported to the garbage dump for incineration, wasting resources and To solve problems such as environmental pollution, provide a comprehensive utilization processing method of Gracilaria that can simultaneously obtain phycoerythrin polypeptide, agar and seaweed insoluble dietary fiber

Method used

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  • Method for comprehensively utilizing and processing gracilaria
  • Method for comprehensively utilizing and processing gracilaria

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] 1) Adjust the pH value of Gracilaria (ratio of material to liquid: 1:10) to 7, add papain with 3% mass of Gracilaria, adjust the temperature to 40° C. and hydrolyze for 8 hours, then filter, and heat the filtrate to 80° C. for 20 minutes. Phycoerythrin polypeptide is obtained after the enzyme is inactivated, concentrated and spray-dried; the physical and chemical indicators of the product are 10.8% moisture, 87.2% protein, and 1.3% fat.

[0028] 2) Add the residue obtained in step 1) to a 6% NaOH solution that is 3 times the wet weight of the residue, adjust the temperature to 90°C for 3 hours, then bleach with an allowed bleaching agent, and add water 8 times the total mass of the original Gracilaria after bleaching , heat up to 95°C and boil the glue for 4 hours, then use a plate and frame filter press to filter, the filtrate is solidified and chopped, then squeezed and dehydrated with an oil press, then dried at 50°C for 6 hours, and finally crushed with a pulverizer ...

Embodiment 2

[0032] 1) Adjust the pH value of Gracilaria (ratio of material to liquid: 1:12) to 9, add trypsin with 4% mass of Gracilaria, adjust the temperature to 38°C and hydrolyze for 7 hours, filter, and heat the filtrate to 80°C for 20 minutes to make Phycoerythrin polypeptide is obtained after the enzyme is inactivated, concentrated and spray-dried; the physical and chemical indicators of the product are 9.8% moisture, 88.0% protein, and 11% fat.

[0033] 2) Add the residue obtained in step 1) to a 7% NaOH solution that is 4 times the wet weight of the residue, adjust the temperature to 95°C for 2.5 hours, then bleach with an allowed bleaching agent, and add 10 times the total mass of the original Gracilaria after bleaching water, heated up to 90°C and boiled for 5 hours, then filtered with a plate and frame filter press, the filtrate was solidified and chopped, then dehydrated with an oil press, dried at 50°C for 6 hours, and finally crushed with a pulverizer to obtain powdered agar...

Embodiment 3

[0036] 1) Adjust the pH value of Gracilaria (material-to-liquid ratio 1:14) to 8, add 4.5% subtilisin of Gracilaria mass, adjust the temperature to 42°C and hydrolyze for 9 hours, filter, and heat the filtrate to 80°C for 20 minutes Inactivate the enzyme, then concentrate and spray-dry to obtain the phycoerythrin polypeptide; the physical and chemical indicators of the product are 9.0% moisture, 89.0% protein, and 11% fat, and the hygienic indicators comply with GB 19643-2005 "Hygienic Standards for Algae Products".

[0037] 2) Add the residue obtained in step 1) to an 8% NaOH solution that is 4.5 times the wet weight of the residue, adjust the temperature to 90°C for 3.0 hours, then bleach with an allowed bleaching agent, and add 12 times the total mass of the original Gracilaria after bleaching Water, warmed up to 95°C and boiled for 4.5 hours, then filtered with a plate and frame filter press, the filtrate was solidified and chopped, then squeezed and dehydrated with an oil ...

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Abstract

A method for comprehensively utilizing and processing asparagus relates to comprehensive utilization of gracilaria. The invention provides a method for comprehensively utilizing and processing gracilaria, through which phycoerythrin polypeptide, agaragar and seaweed insoluble dietary fiber can be obtained simultaneously. The method comprises the following steps: water is added into gracilaria, then protease is added for hydrolization, filtering is performed, the temperature of the filtrate is increased to deactivate enzyme, and phycoerythrin polypeptide and residue are obtained through concentration and spray drying; the obtained residue is treated with aqueous alkali to remove sulfate radical contained in agaragar in the residue, the residue is bleached and water-washed to be neutral, then water is added to boil agaragar, the frond and the agaragar liquid are roughly filtered, and after the rough filtrate is filter-pressed, solidified, chipped, dehydrated through squeezing, dried and crushed, powdery agaragar and frond residue are obtained; after the frond residue is dehydrated through squeezing and dried, seaweed insoluble dietary fiber can be obtained.

Description

technical field [0001] The invention relates to the comprehensive utilization of Gracilaria (also known as asparagus), in particular to a new comprehensive utilization method for simultaneously extracting phycoerythrin polypeptide, agar and seaweed insoluble dietary fiber from Gracilaria. Background technique [0002] At present, Gracilaria is mostly used as a raw material for extracting agar gum, except that it is partially used as abalone feed. At present, most of the techniques for extracting agar from Gracilaria are to use medium-alkali high-temperature method to remove sulfate radicals, then bleach and wash to neutrality, and then directly extract the agar with hot water. This traditional gel extraction method only extracts the agar in the algae, and the phycoerythrin and cellulose in the algae are discharged into the sea as sewage and garbage or transported to the garbage dump for incineration, wasting resources and polluting the environment. Therefore, how to make th...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): A23J1/00C08B37/12A23L1/337A23L1/308A23L17/60
Inventor 许永安
Owner FISHERIES RES INST OF FUJIAN
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