Special nickel-zinc ferrite material for integrated high frequency electrodeless discharge lamp inductive coupler and preparation method
An inductive coupler and nickel-zinc ferrite technology, which is applied in the field of nickel-zinc ferrite materials and preparation for the inductive coupler of an integrated high-frequency electrodeless lamp, can solve the problem of easy generation of electromagnetic radiation, difficulties in product miniaturization, and product heat generation. Concentration and other problems, to achieve the effect of improving electromagnetic loss characteristics, wide pre-burning and sintering temperature range, and good product consistency
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Embodiment 1
[0023] The nickel-zinc ferrite material for the integrated high-frequency electrodeless lamp inductive coupler provided in this embodiment has a main phase of a spinel structure and consists of Fe 2 O 3 , ZnO, NiO and Co 2 O 3 , its composition content is calculated as oxide: Fe 2 O 3 48mol%~56mol%; ZnO is 15mol%~22mol%; NiO is 20mol%~33mol%; Co 2 O 3 0.001 mol% to 0.004 mol%, it also contains 0.05wt% to 0.15wt% of the total weight as a sintering flux, the nano-V that has been surface-modified by a silane coupling agent 2 O 5 ; Nano-MnCO modified with silane coupling agent 3 and CaCO 3 powder as a modification additive, in which nano-MnCO 3 The addition amount is 0.2wt% to 0.5wt% of the total weight; nano-CaCO 3 The addition amount is 0.02wt% to 0.05wt% of the total weight.
[0024] The preparation method of the special nickel-zinc ferrite material for the integrated high-frequency electrodeless lamp inductive coupler provided by this embodiment, the steps are as fo...
Embodiment 2
[0044] 1) Selection of raw materials: the invention provides ultra-wide temperature, high stability and extremely low electromagnetic loss under high frequency and high current, which can be applied to the preparation of nickel-zinc ferrite materials for integrated high-frequency induction lamp power couplers. Raw material selection of industrial pure Fe 2 O 3 , ZnO, NiO and Co 2 O 3 .
[0045] 2) Component design and weighing: according to Fe 2 O 3 56 mol%, ZnO 15 mol%, NiO 28.999 mol% and Co 2 O 3 is 0.001 mol%.
[0046] 3) Mixing of raw materials: put the weighed raw materials into a sand mill, add deionized water, the weight of deionized water is 1.2 times the total weight of the raw materials, and the ball milling time is 2 hours.
[0047] 4) Pre-sintering: Dry the raw materials that have been ball-milled once, and put them into an electric furnace for pre-sintering. The pre-sintering temperature is 1020°C, and the pre-sintering time is 3.5 hours. After pre-sinte...
Embodiment 3
[0057] 1) Selection of raw materials: the invention provides ultra-wide temperature, high stability and extremely low electromagnetic loss under high frequency and high current, which can be applied to the preparation of nickel-zinc ferrite materials for integrated high-frequency induction lamp power couplers. Raw material selection of industrial pure Fe 2 O 3 , ZnO, NiO and Co 2 O 3 .
[0058] 2) Component design and weighing: according to Fe 2 O 3 48 mol%, ZnO 22 mol%, NiO 29.994 mol% and Co 2 O 3 is 0.004 mol%.
[0059] 3) Mixing of raw materials: put the weighed raw materials into a sand mill, add deionized water, the weight of deionized water is 1.2 times the total weight of the raw materials, and the ball milling time is 1 hour.
[0060] 4) Pre-sintering: Dry the raw materials that have been ball-milled once, and put them into an electric furnace for pre-sintering. The pre-sintering temperature is 1180°C, and the pre-sintering time is 1.5 hours. After pre-sinter...
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