Method of preparing low-density well cementation cement check block of oil well by utilizing silicon carbide ceramic microbeads

Abstract

The invention provides a method of preparing a low-density well cementation cement check block of an oil well by utilizing silicon carbide ceramic microbeads. The method comprises the following steps: preparing silicon carbide closed-hole hollow ceramic microbeads; burdening; mixing; stirring and mixing; carrying out mould testing; carrying out a strength test. The method is characterized by specifically comprising the following steps: stirring and mixing 40-50wt% of G-grade well cementation cement, 10-15wt% of 13-micron superfine cement, 25-35wt% of closed-hole silicon carbide ceramic microbeads with the grain size of 5-50 microns, 5-7wt% of coal ash with the loss on ignition of 1.1%, 1.5-2wt% of calcium oxide with the purity of 99.9%, 0.5-1.0wt% of sodium sulfate and 1-3wt% of micro-silicon in a stirrer for 40 seconds in a micro-silicon of 0.5-0.6(W / C); pouring and carrying out mould testing; maintaining for 24 hours and 48 hours in a water bath maintaining box at a constant temperature of 52 DEG C; soaking for 1 hour in cold water after demoulding and carrying out performance test.

Description

technical field

[0001] The invention relates to a method for preparing a low-density oil well cementing cement test block by using silicon carbide closed-pore hollow ceramic microspheres, which belongs to the field of material technology. Background technique

[0002] At present, the domestic cementing lightening agent uses floating beads in fly ash, including sinking beads and floating beads in fly ash, and the density of sinking beads is 1.1-2.8g / cm 3 , between, and the content accounts for 30-70% of fly ash. Floating beads are glass beads in fly ash that are less dense than water. Floating beads mainly include aluminosilicate glass beads and porous carbon particles. Floating beads after removing carbon particles It mainly includes thin-walled aluminosilicate glass beads with smooth inner and outer surfaces and large volume. 0.5 to 1% of the total ash, and the aluminosilicate glass microspheres are hollow spheres.

[0003] Among them, the floating beads in the fly ash a...