A photostable sunscreen composition
A composition and light-resistant technology, which can be used in skin care preparations, medical preparations containing active ingredients, cosmetics, etc., and can solve the problems of low stability and poor stability.
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Embodiment 1 to 4
[0055] Examples 1 to 4: Photostability of compositions according to the invention compared to compositions outside the invention
[0056] Several compositions shown in Table 1 were prepared. The steps for preparing the salvia miltiorrhiza extract (embodiment 3) are as follows:
[0057] The aqueous ethanolic extract of Salvia miltiorrhiza (50 g) was redissolved in distilled water (1 L) at 45-50° C. by stirring for 15 minutes. The resulting suspension was extracted with ethyl acetate (200ml x 5). by Na 2 SO 4 The ethyl acetate layer was collected and dried on a rotary evaporator. About 10 g of dry powder are obtained.
[0058] Table 1
[0059]
[0060] #The Danshen extract used was analyzed to contain ~2.0% Tanshinone IIA. The concentration of tanshinone IIA in the extract was determined by silica gel chromatography in Comniflash and elution with gradient increments of ethyl acetate-hexane.
[0061] Procedure for determining the photostability of dibenzoylmethane c...
Embodiment 5 to 6
[0069] Examples 5 to 6: Demonstration of pure Tanshinone IIA as a photostabilizer for Parsol-1789
[0070] The efficacy of Tanshinone IIA for photostabilization of the UV-A sunscreen Parsol-1789, a dibenzoylmethane compound, was demonstrated in chloroform solution at a concentration of 5 ppm. Example 5 is a solution containing only 5 ppm Parsol-1789, while Example 6 contains 5 ppm each of Parsol-1789 and Tanshinone IIA. In Example 5, pure tanshinone IIA was extracted from the plant Salvia miltiorrhiza using the following steps;
[0071] An alcoholic aqueous extract of Salvia miltiorrhiza was first prepared by placing the root (50 g) of the plant Salvia miltiorrhiza in a 95% ethanol / water mixture at a weight ratio of root to mixture of 1:20. The extract was then redissolved in distilled water (1 L) at 45-50° C. by stirring for 15 minutes. Fractions of interest were fractionated with ethyl acetate and water. The ethyl acetate fractions were dried on a rotary evaporator. Th...
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