Adsorbent with adsorption and oxidation synergistic effects on indoor toluene and preparation method and application of adsorbent
A synergistic and adsorbent technology, applied in the field of indoor air purification, can solve problems such as poor stability, adsorbents are easily affected by the environment, and large absorption devices, and achieve the effects of low cost, high adsorption rate, and broad application prospects
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Embodiment 1
[0032] Investigation on the concentration of potassium permanganate:
[0033] The preparation method of the adsorbent having the synergistic effect of adsorption and oxidation on indoor toluene comprises the following steps:
[0034] A. Potassium permanganate and spherical H-ZSM-5 molecular sieve (silicon-aluminum ratio: 70-80) are 1:1 by mass ratio and the mass concentration of potassium permanganate is 1%, 2%, 3%, 4% respectively. %, 5%, 10%, 50% absolute ethanol solution for 5 hours ultrasonic immersion;
[0035] B. In step A, the impregnated H-ZSM-5 molecular sieve is placed in a nitrogen blowing device for drying, and the sample is purged at room temperature until it is completely dry by controlling the nitrogen gas flow rate of 0.02L / min, and the indoor Toluene is an adsorbent that has a synergistic effect of adsorption and oxidation.
[0036] Among them, when the mass concentration of potassium permanganate is 5%, this kind of adsorbent that has a synergistic effect o...
Embodiment 2
[0042] Investigation of the time of impregnation:
[0043] The preparation method of the adsorbent having the synergistic effect of adsorption and oxidation on indoor toluene comprises the following steps:
[0044] A. Ultrasonic impregnation of potassium permanganate and spherical H-ZSM-5 (silicon-aluminum ratio: 70-80) molecular sieves in an absolute ethanol solution with a mass ratio of 1:1 and potassium permanganate mass concentration of 5%. 1 hour, 4 hours, 10 hours respectively;
[0045] B. In step A, the impregnated H-ZSM-5 molecular sieve is placed in a nitrogen blower for drying, and the sample is purged to completely dry at room temperature by controlling the nitrogen gas flow rate of 0.1L / min, and the indoor Toluene is an adsorbent that has a synergistic effect of adsorption and oxidation.
[0046] Wherein, when the immersion time is 4 hours, this kind of adsorbent that has the synergistic effect of adsorption and oxidation on indoor toluene includes potassium perm...
Embodiment 3
[0052] Investigation on the ratio of silicon to aluminum in H-ZMS-5 molecular sieve:
[0053] The preparation method of the adsorbent having the synergistic effect of adsorption and oxidation on indoor toluene comprises the following steps:
[0054] A. Spherical H-ZSM-5 molecular sieves with different ratios of potassium permanganate and silicon to aluminum were impregnated ultrasonically for 4 hours in an absolute ethanol solution with a mass ratio of 1:1 and a mass concentration of potassium permanganate of 5%. The ratio of silicon to aluminum in H-ZSM-5 is 18-30, 70-80, 100-120 respectively.
[0055] B. Place the H-ZSM-5 molecular sieve impregnated in step A in a nitrogen blower for drying. By controlling the nitrogen gas flow rate of 0.05L / min, the sample is purged until completely dry at room temperature, and the indoor toluene is obtained. Adsorbents with synergistic effects of adsorption and oxidation.
[0056] Among them, when the ratio of silicon to aluminum in H-ZS...
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