Method for preparing cockroach insecticide tablets by Sichuan pepper essential oil

A technology of prickly ash essential oil and cockroaches, which is applied in the field of preparation of insect repellent drugs, can solve the problems of not truly reflecting the repellency of cockroaches to drugs, and achieve the effects of low cost, simple preparation process, and various applicable environments

Inactive Publication Date: 2015-01-07
FUJIAN NORMAL UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

One of the reasons may be that most of the current research uses the filter paper immersion method, which tests the short-term respo...

Method used

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  • Method for preparing cockroach insecticide tablets by Sichuan pepper essential oil
  • Method for preparing cockroach insecticide tablets by Sichuan pepper essential oil
  • Method for preparing cockroach insecticide tablets by Sichuan pepper essential oil

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0021] formula

[0022]

[0023] preparation

[0024] 1. Put 100g of Zanthoxylum bungeanum in the refrigerator for 8 hours, crush it with a pulverizer, pass through a 40-mesh sieve, add 100ml of distilled water, soak for 4 hours, and extract by steam distillation to obtain the Zanthoxylum bungeanum essential oil extract for later use.

[0025] The temperature used in the steam distillation method is 110°C.

[0026] 2. First mix 400ml of absolute ethanol and 100 Tween 80 evenly, then add 15ml of Zanthoxylum bungeanum essential oil extract, mix well to make Zanthoxylum bungeanum essential oil insect repellent slow-release agent.

[0027] 3. Add 450ml of distilled water to 150g of agar, and heat to dissolve the agar completely. When the agar solution is cooled to 45°C, add the essential oil insect repellent slow-release solution prepared in step 2 of 60 to the agar solution, and stir while adding, so that The essential oil insect repellent sustained-release liquid is mixed e...

Embodiment 2

[0032] formula

[0033]

[0034] preparation

[0035] 1. Put 300g of Chinese prickly ash in the refrigerator for 8 hours, crush it with a pulverizer, pass through a 40-mesh sieve, add 300ml of distilled water, soak for 3 hours, and use steam distillation to extract the Chinese prickly ash essential oil extract for later use.

[0036] The temperature used in the steam distillation method is 100°C.

[0037] 2. First mix 1600ml of absolute ethanol and 400ml of Tween 80 evenly, then add 40ml of Zanthoxylum bungeanum essential oil extract, mix well to make Zanthoxylum bungeanum essential oil insect repellent slow-release agent.

[0038] 3. Add 1200ml of distilled water to 400g of agar, and heat to dissolve the agar completely. When the agar solution is cooled to 35°C, take 40ml of the essential oil deworming slow-release solution prepared in step 2 and add it to the agar solution. Stir while adding to make the essential oil The insect repellent sustained-release solution is mi...

Embodiment 3

[0043] formula

[0044]

[0045]

[0046] preparation

[0047] 1. Put 100g of Zanthoxylum bungeanum in the refrigerator for 8 hours, crush it with a pulverizer, pass through a 40-mesh sieve, add 100ml of distilled water, soak for 2 hours, and extract by steam distillation to obtain the Zanthoxylum bungeanum essential oil extract for later use.

[0048] The temperature adopted in the steam distillation method is 105°C.

[0049] 2. First mix 2000ml absolute ethanol and 500ml Tween 80 evenly, then add pepper essential oil extract, mix well to make pepper essential oil deworming slow-release liquid.

[0050]3. Add 1895ml of distilled water to 650g of agar, and heat to dissolve the agar completely. When the agar solution is cooled to 50°C, take 60ml of the essential oil deworming slow-release solution prepared in step 2 and add it to the agar solution, and stir while adding to make the essential oil The insect repellent sustained-release solution is mixed evenly with the ag...

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Abstract

The invention relates to a method for preparing cockroach insecticide tablets by Sichuan pepper essential oil. The method comprises the following steps: crushing Sichuan pepper by utilizing a crusher according to a ratio of 10ml to 15ml of a Sichuan pepper essential oil extract liquid, 400ml of absolute ethyl alcohol, 100ml of tween 80 and 100g to 150g of agar, adding distilled water to soak the crushed Sichuan pepper, and extracting the Sichuan pepper essential oil extract liquid for standby use in a vapor distilling method; uniformly mixing the absolute ethyl alcohol and tween 80, and then adding the Sichuan pepper essential oil extract liquid to obtain the Sichuan pepper essential oil insecticide slow-release preparation; adding the agar into the distilled water, heating and dissolving the agar, cooling the agar, and slowly adding the essential oil insecticide slow-release agent prepared in the step 2 into the agar solution, heating and stirring the mixed solution, uniformly mixing the mixed solution, and slowly pouring the mixed solution into a hollow cylindrical forming mold to prepare a cylindrical round bar; cutting the cylindrical round bar into tablets; and applying the glue on one side of each tablet to prepare the cockroach insecticide tablet. The method is simple in preparation process, low in cost and diversified in applicable environments, and the repellent rate of the prepared cockroach insecticide tablet for American cockroach and German cockroach can reach 88 to 100 percent.

Description

technical field [0001] The invention relates to a method for preparing an insect-repelling tablet with the function of repelling cockroaches from prickly ash essential oil, and belongs to the technical field of preparation of anthelmintic drugs. Background technique [0002] Cockroach belongs to Insecta, Blattata, is a class of insects with a long history, and original cockroach appeared on the earth in the Silurian Period about 400,000,000 years ago. At present, there are mainly Periplaneta americana, Blattella germanica, Blattella black breast, Periplaneta australis and Periplaneta japonica that are closely related to human life. The most common ones in China are Periplaneta americana and Blattella germanica. [0003] Cockroaches not only spread diseases, but also often bite other items, such as cotton and wool products, leather products, paper, books, etc. Therefore cockroach is not only a kind of sanitation pest, but also file pest and textile pest. Cockroaches also of...

Claims

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Application Information

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IPC IPC(8): A01N65/36A01N25/34A01P17/00
CPCY02A50/30
Inventor 王正朝肖义军林尧林雅红林丽红
Owner FUJIAN NORMAL UNIV
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