A kind of microbial water purifying agent for vannamei cultured water and preparation method thereof
A technology for microbial reagents and aquaculture water, applied in biological water/sewage treatment, chemical instruments and methods, water/sludge/sewage treatment, etc., can solve problems such as water quality decline, production decline, and shrimp incidence increase, and achieve purification High efficiency and easy precipitation effect
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Embodiment 1
[0024] (1) Preparation of magnetic silicon spheres with surface-modified C8 and C18 alkyl chains:
[0025] (1-1) Synthesis of Fe by hydrothermal method 3 o 4 Magnetic nanoparticles: 1 g of FeCl 3 ·6H 2 O, dissolved in 30ml of ethylene glycol, adding 4 grams of anhydrous sodium acetate, the reaction temperature is 200 ° C, the reaction time is 12 hours, and Fe is generated 3 o 4 magnetic nanoparticles;
[0026] (1-2) the above Fe 3 o 4 Wash the magnetic nanoparticles with water to remove water-soluble impurities, and then disperse them in 10 g of water to obtain dispersion A. Take a centrifuge tube, add 3 g of the above dispersion A, add 5 ml of 2M HCl solution and sonicate for 8 minutes, and then separate and remove the green clear liquid with a magnet. Then disperse with 10ml of water, collect the particles with a magnet, remove the light green clear liquid, disperse with 5ml of 10wt% trisodium citrate solution ultrasonically, let stand for 2h, and disperse with 5ml of...
Embodiment 2
[0033] Basically the same as in Example 1, the microbial water purifying agent used for the culture water of Penaeus vannamei was prepared, the only difference being that the surface modifier was different in step (1-4). In Example 2, 0.3 g of dimethyloctylsilane was used as the surface modifier.
Embodiment 3
[0035] Basically the same as in Example 1, the microbial water purifying agent used for the culture water of Penaeus vannamei was prepared, the only difference being that the surface modifier was different in step (1-4). In Example 3, 0.3 g of octadecyltriethoxysilane was used as the surface modifier.
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