Microorganism water-purifying agent used for culture water of penaeus vannamei boone, and preparation method thereof
A microbial reagent, aquaculture water technology, applied in biological water/sewage treatment, chemical instruments and methods, water/sludge/sewage treatment, etc. High efficiency and easy precipitation effect
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Embodiment 1
[0024] (1) Preparation of magnetic silica spheres with surface-modified C8 and C18 alkyl chains:
[0025] (1-1) Synthesis of Fe by hydrothermal method 3 o 4 Magnetic nanoparticles: 1 g of FeCl 3 ·6H 2 O, dissolved in 30ml of ethylene glycol, adding 4 grams of anhydrous sodium acetate, the reaction temperature is 200 ° C, the reaction time is 12 hours, and Fe is generated 3 o 4 magnetic nanoparticles;
[0026] (1-2) The above Fe 3 o 4 Wash the magnetic nanoparticles with water to remove water-soluble impurities, and then disperse them in 10 g of water to obtain dispersion A. Take a centrifuge tube, add 3 g of the above dispersion A, add 5 ml of 2M HCl solution and sonicate for 8 minutes, and then use a magnet to separate and remove the green color. Clear liquid, then disperse with 10ml water, collect particles with magnet, remove light green clear liquid, disperse ultrasonically with 5 ml 10wt% trisodium citrate solution, let it stand for 2 hours, re-disperse with 5 ml w...
Embodiment 2
[0033] Basically the same as in Example 1, the microbial water purifying agent for the culture water of Penaeus vannamei was prepared, the only difference being that the surface modification agent in step (1-4) was different. In Example 2, 0.3 g of dimethyloctylsilane was used as the surface modifier.
Embodiment 3
[0035]Basically the same as in Example 1, a microbial water purifying agent for the culture water of Penaeus vannamei was prepared, the only difference being that the surface modification agent in step (1-4) was different. In Example 3, 0.3 g of octadecyltriethoxysilane was used as the surface modifier.
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