A kind of automatic intelligent production device for preparing single-layer graphene by chemical method

A single-layer graphene and intelligent production technology, which is applied in the field of automatic intelligent production devices for the preparation of single-layer graphene by chemical methods, can solve problems such as lack of intelligent control, restrict development and application, and immature technology and technology, and achieve stable product quality , improve competitiveness, and enhance the effect of clean production image

Active Publication Date: 2016-10-05
QINGDAO HUAGAO GRAPHENE CORP LTD
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0002] Graphene is a new material with a single-layer sheet structure composed of carbon atoms. It is the thinnest and hardest nanomaterial known in the world. It has extraordinary electrical conductivity, thermal conductivity, strength and Excellent light transmission, can be widely used in solar cells, sensors, nanoelectronics, high-performance electronic devices, composite materials, field emission materials, gas sensors and energy storage, etc. However, problems such as low output, high cost, and poor quality of graphene seriously restrict its development and application
At present, graphene is still in the stage of research and development, pilot test, and small batch production. Industrial production has immature technology and process, and there is no intelligently controlled production line.

Method used

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  • A kind of automatic intelligent production device for preparing single-layer graphene by chemical method

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Embodiment

[0015]The main structure of this embodiment includes a center console 1, a pre-oxidation reaction kettle 2, a first decanter centrifuge 3, a double-cone rotary vacuum dryer 4, a spray dryer 5, an industrial microwave heating reduction furnace 6, and a sewage treatment system 7 , the first chromatographic control device 8, the first pH sensor 9, the temperature sensor 10, the first dry humidity sensor 11, the photoelectric sensor 12, the time relay 13, the pressure temperature and vacuum sensor 14, the first solenoid valve 15, the first Control element 16, second control element 17, second solenoid valve 18, third control element 19, fourth control element 20, fifth control element 21, oxidation reactor 22, second chromatography control device 23, second photoelectric sensor 24. The second solenoid valve 25, the sixth control element 26, the second decanter centrifuge 27, the second pH sensor 28, the seventh control element 29, the eighth control element 30, the second pressure ...

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Abstract

The invention belongs to the technical field of equipment for preparing single-layer graphene by a chemical method, and relates to an automatic intelligent production device for preparing single-layer graphene by the chemical method. The upper part of a pre-oxidization reaction kettle is connected with a first chromatography control device; the upper part of the first chromatography control device is connected with a first photoelectric sensor; the upper part of a first horizontal screw centrifuge is connected with a first pH sensor; the upper part of a double-tapered rotary vacuum drying tank is connected with a temperature sensor and a first humidity sensor; the upper part of an oxidization reaction kettle is connected with a second chromatography control device; the upper part of the second chromatography control device is connected with a second photoelectric sensor; the upper part of a second horizontal screw centrifuge is connected with a second pH sensor and a time relay; the upper part of a spray dryer is connected with a second humidity sensor; and the upper part of an industrial microwave heating reduction furnace is connected with a second pressure temperature and vacuum degree sensor. The automatic intelligent production device is reasonable in structure, reliable in principle, environmentally-friendly, low in cost and high in degree of automation.

Description

Technical field: [0001] The invention belongs to the technical field of equipment for preparing single-layer graphene by chemical method, and relates to an automatic intelligent production device for preparing single-layer graphene by chemical method, which is suitable for large-scale production of single-layer graphene, and its automatic intelligent system adopts the element control of the preparation process unit According to the step process of chemical preparation of single-layer graphene, the connection of each unit is automatically completed until the required products of graphene oxide aqueous dispersion, graphene oxide powder and single-layer graphene powder are prepared. Background technique: [0002] Graphene is a new material with a single-layer sheet structure composed of carbon atoms. It is the thinnest and hardest nanomaterial known in the world. It has extraordinary electrical conductivity, thermal conductivity, strength and Excellent light transmission, can b...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C01B31/04
Inventor 郭洪云王福山施建新钟成钱锋潘东晓
Owner QINGDAO HUAGAO GRAPHENE CORP LTD
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