Fruit freshness-keeping fruit wax and preparation method thereof
A fruit wax and fruit technology, which is applied in the protection of fruits/vegetables with a protective layer, the preservation of food ingredients as antimicrobial agents, and the use of food ingredients as coating agents, etc. insecurity, etc.
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Embodiment 1
[0018] The invention provides a kind of morpholine fatty acid ester salt, is prepared from phottoic acid (bleached shellac), abietic acid resin (PL-101, conforms to SGS), morpholine, ethanol, ammonia water and deionized water, the obtained The weight ratio of the above-mentioned photic acid (bleached shellac), abietic acid resin (PL-101, conforming to SGS), morpholine, ethanol, ammonia water and deionized water is 10.0~18.0:5.0~15.0:1.93~3.95:8.0 ~10.0: 0.5~1.2: 60.0~70.0, first add ethanol and 3~20% deionized water into a reaction kettle, preheat to 65~73℃, put in eucalyptus acid and abietic acid resin, raise the temperature to 76 ~83℃, add 70~80% morpholine, stir for 10~30min, apply pressure, heat up to 85~93℃, keep warm for 1~5 hours, cool down to 73~83℃, add remaining morpholine, ammonia water and remaining deionized water, continue to stir for 20 to 35 minutes, open the kettle and cool to 20 to 50°C, and filter to obtain morpholine fatty acid ester salt.
Embodiment 2
[0020] The present invention also provides a kind of phototungate ester salt, which is prepared from phototallow acid (bleached shellac), morpholine, ethanol, ammonia water and deionized water. The weight ratio of morphine, ethanol, ammonia water and deionized water is 10.0~18.0: 1.93~3.95: 8.0~10.0: 0.5~1.2: 60.0~70.0, first add ethanol and 3~20% deionized water into a reaction kettle , preheat to 65-73°C, put in eutrophic acid, raise the temperature to 76-83°C, add 70-80% morpholine, stir for 10-30min, apply pressure, heat up to 85-93°C, keep warm for 1-5 Hours, lower the temperature to 73-83°C, add the remaining morpholine, ammonia water and the remaining deionized water, continue to stir for 20-35 minutes, open the kettle and cool to 20-50°C, and filter to obtain the phospholipidate salt.
Embodiment 3
[0022] The present invention also provides a silicone acrylic resin, which is prepared from acrylic acid or acrylate, propylene silicone, potassium persulfate, isopropanol, ammonia water and deionized water. The acrylic acid or acrylate, propylene silicone, The weight ratio of potassium persulfate, isopropanol, ammonia water and deionized water is 20~25: 0.5~1.5: 0.3~0.6: 10.0~16.0: 3.0~5.0: 60.0~66.0, first deionized water and isopropanol Put it into a reaction kettle for heating, preheat to 65~75℃, add 5~15% K 2 S 2 o 8 , and then heated to 76 ~ 85 ° C, began to drop acrylic acid or acrylate, acrylic silicone and 70 ~ 83% of K 2 S 2 o 8 , keep warm at 82-85°C for 2-3 hours, add the remaining K after the dropwise reaction 2 S 2 o 8 , kept at 85`90°C for 0.5-1.5 hours, then cooled to 60-75°C, added ammonia water to adjust the pH to 7-8, continued to cool down to 20-50°C, and filtered to obtain silicone acrylic resin.
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