Compound taxus chinensis boil-free granules as well as preparation method and application thereof
A technology of compound yew and decoction-free granules, which is applied in the field of compound yew decoction-free granules and its preparation, can solve the problems of complex process, destruction of active ingredients, and low dissolution rate, and achieve simple preparation, high bioavailability, and promotion The effect of sebum metabolism
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Embodiment 1
[0047] A preparation method of compound yew decoction-free granules, comprising the following steps:
[0048] (1) Take the southern yew (twigs, leaves), raw barley, salvia miltiorrhiza, Phellodendron chinensis, purple peony root, Patina, Folium Folium, dandelion, Anemarrhena anemarrhena, scutellaria baicalensis, honeysuckle, Alisma, centipede, dried, smash. Pass through a 80-mesh sieve, and the under-sieve is ready for use.
[0049] (2) Take 10kg of the undersieve, put it into an ultrasonic wall breaking extraction tank, add 15 times of water, fully stir and soak at 50°C for 1 hour.
[0050] (3) Using high-power ultrasonic generator, power 15-30kW, frequency 20-25kHZ, sound intensity 2W / cm 2 , sonicated for 30 minutes.
[0051] (4) Transfer the feed solution after ultrasonic wall breaking to a stirring extraction tank, add 0.3% (g / g) neutral protease, adjust the pH to 6.8, and perform enzymatic hydrolysis for 90 minutes. Hydrolyzes free proteins in glycoproteins and glycan...
Embodiment 2
[0057] A preparation method of compound yew decoction-free granules, comprising the following steps:
[0058] (1) Take the southern yew (twigs, leaves), raw barley, salvia miltiorrhiza, Phellodendron chinensis, purple peony root, Patina, Folium Folium, dandelion, Anemarrhena anemarrhena, scutellaria baicalensis, honeysuckle, Alisma, centipede, dried, smash. Pass through a 80-mesh sieve, and the under-sieve is ready for use.
[0059] (2) Take 10kg of the undersieve, put it into an ultrasonic wall breaking extraction tank, add 15 times of water, fully stir and soak at 50°C for 1 hour.
[0060] (3) Using high-power ultrasonic generator, power 15-30kW, frequency 20-25kHZ, sound intensity 2W / cm 2 , sonicated for 40 minutes.
[0061] (4) Transfer the feed solution after ultrasonic wall breaking to a stirring extraction tank, add 0.5% (g / g) neutral protease, adjust the pH to 7.0, and perform enzymatic hydrolysis for 90 minutes. Hydrolyzes free proteins in glycoproteins and glycan...
Embodiment 3
[0067] A preparation method of compound yew decoction-free granules, comprising the following steps:
[0068] (1) Take the southern yew (twigs, leaves), raw barley, salvia miltiorrhiza, Phellodendron chinensis, purple peony root, Patina, Folium Folium, dandelion, Anemarrhena anemarrhena, scutellaria baicalensis, honeysuckle, Alisma, centipede, dried, smash. Pass through a 80-mesh sieve, and the under-sieve is ready for use.
[0069] (2) Take 10kg of the undersieve, put it into an ultrasonic wall breaking extraction tank, add 15 times of water, fully stir and soak at 50°C for 1 hour.
[0070] (3) Adopt high-power ultrasonic generator, power 15-30kW, frequency 20-25kHZ, sound intensity 3W / cm 2 , sonicated for 30 minutes.
[0071] (4) Transfer the feed solution after ultrasonic wall breaking to a stirring extraction tank, add 0.8% (g / g) neutral protease, adjust the pH to 6.9, and perform enzymatic hydrolysis for 90 minutes. Hydrolyzes free proteins in glycoproteins and glycan...
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