Environment-friendly long-acting type nano-silver base wood and bamboo material antibacterial mould inhibitor and preparing method and application thereof
A kind of technology of antibacterial and antifungal agent and nano silver
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Embodiment 1
[0050] 1. Preparation of nano silver-based antibacterial and antifungal agent for wood and bamboo
[0051] Under room temperature environment, 0.25g carboxymethyl chitosan (the degree of carboxymethyl substitution is 91%, the degree of deacetylation is 90%, the weight average molecular weight is 100,000) is dissolved in deionized water, and on the magnetic stirrer Stir for 10 min at a rotating speed of 1000 rpm to obtain a carboxymethyl chitosan solution with a concentration of 0.1 wt%. 0.17g of silver nitrate and 0.18g of glucose were respectively dissolved in deionized water to obtain a silver salt solution and a reducing agent solution with a concentration of 1 wt%.
[0052] The evenly stirred carboxymethyl chitosan solution was placed in a microwave radiation instrument, the microwave radiation power was adjusted to 900W, and the radiation temperature was 80°C. Under the condition of microwave radiation, slowly drop the silver salt solution into the carboxymethyl chitosan...
Embodiment 2
[0058] 1. Preparation of nano silver-based antibacterial and antifungal agent for wood and bamboo
[0059] Under room temperature environment, 1g carboxymethyl chitosan (the carboxymethyl substitution degree is 95%, the degree of deacetylation is 95%, the weight average molecular weight is 50,000) is dissolved in deionized water, and on the magnetic stirrer with Rotate at 1500 rpm, stir for 20 min to obtain a carboxymethyl chitosan solution with a concentration of 0.5 wt%. 0.34g of silver nitrate and 0.72g of fructose were dissolved in deionized water respectively to obtain a silver salt solution and a reducing agent solution with a concentration of 1 wt%.
[0060] The evenly stirred carboxymethyl chitosan solution was placed in a microwave radiation instrument, the microwave radiation power was adjusted to 600W, and the radiation temperature was 70°C. Under the condition of microwave radiation, the silver salt solution was slowly dropped into the carboxymethyl chitosan solut...
Embodiment 3
[0065] 1. Preparation of nano silver-based antibacterial and antifungal agent for wood and bamboo
[0066] Under room temperature environment, 1g carboxymethyl chitosan (the degree of carboxymethyl substitution is 80%, the degree of deacetylation is 85%, the weight average molecular weight is 20,000) is dissolved in deionized water, and on the magnetic stirrer Rotate at 1500 rpm and stir for 20 min to obtain a carboxymethyl chitosan solution with a concentration of 1 wt%. 0.34g of silver nitrate and 0.36g of glucose were respectively dissolved in deionized water to obtain a silver salt solution and a reducing agent solution with a concentration of 0.5wt%.
[0067] The evenly stirred carboxymethyl chitosan solution was placed in a microwave radiation instrument, the microwave radiation power was adjusted to 800W, and the radiation temperature was 60°C. Under the condition of microwave radiation, the silver salt solution was slowly dropped into the carboxymethyl chitosan soluti...
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