Adhesive composition, adhesive, adhesive sheet, and display body
A technology of adhesion and composition, applied in the direction of adhesive types, cyclodextrin adhesives, ester copolymer adhesives, etc., can solve the problems of light reflection loss, etc., achieve excellent step followability, high film the effect of strength
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
preparation example Construction
[0089] (5) Preparation of adhesive composition
[0090] The adhesive composition P can be produced by preparing the (meth)acrylate polymer (A), and mixing the obtained (meth)acrylate polymer (A) and the polyrotaxane compound (B) , isocyanate crosslinking agent (C), and add additives according to need.
[0091] The (meth)acrylate polymer (A) can be produced by polymerizing a mixture of monomers constituting a polymer by a normal radical polymerization method. It is preferable to perform polymerization of a (meth)acrylate polymer (A) by the solution polymerization method using a polymerization initiator as needed. Examples of the polymerization solvent include ethyl acetate, n-butyl acetate, isobutyl acetate, toluene, acetone, hexane, methyl ethyl ketone, and the like, and two or more of them may be used in combination.
[0092] Examples of the polymerization initiator include azo compounds, organic peroxides, and the like, and two or more types may be used in combination. Ex...
Embodiment 1
[0152] 1. Preparation of (meth)acrylate polymer
[0153] Copolymerize 60 parts by mass of 2-ethylhexyl acrylate, 20 parts by mass of isobornyl acrylate, 5 parts by mass of 4-acryloylmorpholine, and 15 parts by mass of 2-hydroxyethyl acrylate to prepare a (meth)acrylate polymer (A). As a result of measuring the molecular weight of this (meth)acrylate polymer (A) by the method mentioned later, the weight average molecular weight (Mw) was 600,000.
[0154] 2. Preparation of Adhesive Composition
[0155]100 parts by mass of the (meth)acrylate polymer (A) obtained in the above step 1 (solid content conversion value; hereinafter the same), polyrotaxane compound (B) (manufactured by Advanced Softmaterials Inc., product name "CELM High Polymer SH3400P", linear molecule: polyethylene glycol, cyclic molecule: α-cyclodextrin with hydroxypropyl and caprolactone chains, protecting group: adamantyl, weight average molecular weight (Mw) 700,000 , hydroxyl value 72 mgKOH / g) 3.0 parts by ma...
Embodiment 2~15
[0175] [Examples 2-15, Comparative Examples 1-5]
[0176] In addition to the types and ratios of the monomers constituting the (meth)acrylate polymer (A), the weight average molecular weight of the (meth)acrylate polymer (A), the addition amount of the polyrotaxane compound (B), The kind and addition amount of the isocyanate crosslinking agent (C) and the addition amount of the silane coupling agent were changed to those shown in Table 1, and it carried out similarly to Example 1, and produced the adhesive sheet.
[0177] However, the weight average molecular weight (Mw) is a weight average molecular weight in terms of polystyrene measured using gel permeation chromatography (GPC) under the following conditions (GPC measurement).
[0178]
[0179] ・GPC measuring device: HLC-8020 manufactured by TOSOH CORPORATION
[0180] ・GPC column (passed in the following order): manufactured by TOSOH CORPORATION
[0181] TSK guard column HXL-H
[0182] TSK gel GMHXL (×2)
[0183] TSK ...
PUM
Property | Measurement | Unit |
---|---|---|
glass transition temperature | aaaaa | aaaaa |
thickness | aaaaa | aaaaa |
thickness | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com