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Lightweight bauxite refractory aggregate containing micro-closed pores and preparation method thereof

A refractory aggregate and air-closed technology, which is applied in the field of refractory materials, can solve the problems of inability to resist erosion and penetration of slag and high-temperature media, complex wet preparation process, low apparent porosity and pore size, and promote grain boundary movement rate, reducing the apparent porosity, and the effect of small pore size

Active Publication Date: 2019-07-09
WUHAN UNIV OF SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, with the above preparation methods, the raw materials are ground and reshaped. On the one hand, the process is more complicated. More importantly, the prepared refractory aggregate usually has a high apparent porosity and a large pore size, and cannot resist slag during use. And the erosion and penetration of high temperature medium
[0005] "A microporous lightweight bauxite refractory aggregate and its preparation method" (ZL 201410447797.X) patent technology, a microporous lightweight bauxite refractory aggregate was prepared by a wet method. Although the prepared product has relatively Low apparent porosity and pore size, but the wet preparation process used is relatively complicated, and it is difficult to realize industrial production

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] A lightweight bauxite refractory aggregate containing micro-closed pores and a preparation method thereof. The preparation method described in this embodiment is:

[0023] Put the lumpy bauxite raw material in a microwave device, raise the temperature to 950°C with a microwave segmental heating method at a heating rate of 20-60°C / min, and cool naturally to room temperature to obtain a pre-fired billet. The method of heating up to 950°C by the microwave segmental heating method is: use microwave heating, when the temperature of the microwave device rises to 350°C, 450°C, 550°C, 650°C and 950°C respectively, keep warm for 5-20°C minute;

[0024] Then transfer the pre-fired billet into a high-temperature kiln, and use the kiln step-by-step heating method to raise the temperature to the final temperature at a heating rate of 3-7°C / min to obtain light-weight bauxite with slightly closed pores. Refractory aggregate. The stepwise heating up method of the kiln to the final t...

Embodiment 2

[0028] A lightweight bauxite refractory aggregate containing micro-closed pores and a preparation method thereof. The preparation method described in this embodiment is:

[0029] Put the lumpy bauxite raw material in a microwave device, raise the temperature to 950°C with a microwave segmental heating method at a heating rate of 20-60°C / min, and cool naturally to room temperature to obtain a pre-fired billet. The method of heating up to 950°C by the microwave segmental heating method is: use microwave heating, when the temperature of the microwave device rises to 350°C, 450°C and 550°C respectively, keep warm for 5-20 minutes, when the microwave When the temperature of the device rises to 650°C and 950°C respectively, keep warm for 15 to 30 minutes.

[0030] Then transfer the pre-fired billet into a high-temperature kiln, and use the kiln step-by-step heating method to raise the temperature to the final temperature at a heating rate of 3-7°C / min to obtain light-weight bauxite...

Embodiment 3

[0034] A lightweight bauxite refractory aggregate containing micro-closed pores and a preparation method thereof. The preparation method described in this embodiment is:

[0035] Put the lumpy bauxite raw material in a microwave device, raise the temperature to 950°C with a microwave segmental heating method at a heating rate of 20-60°C / min, and cool naturally to room temperature to obtain a pre-fired billet. The method of heating up to 950°C by the microwave segmental heating method is: use microwave heating, when the temperature of the microwave device rises to 350°C, 450°C and 550°C respectively, keep warm for 5-20 minutes, when the microwave When the temperature of the device rises to 650°C and 950°C respectively, keep warm for 15 to 30 minutes.

[0036] Then transfer the pre-fired billet into a high-temperature kiln, and use the kiln step-by-step heating method to raise the temperature to the final temperature at a heating rate of 3-7°C / min to obtain light-weight bauxite...

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Abstract

The invention relates to a lightweight bauxite refractory aggregate containing micro-closed pores and a preparation method thereof. The technical solution is: put the lumpy bauxite raw meal in a microwave device, and heat up at a heating rate of 20-100°C / min. When the temperature of the microwave device rises to 350°C, 450°C, 550°C, 650 ℃ and 950 ℃, keep warm for 5 to 30 minutes each, and naturally cool to room temperature to obtain a pre-fired billet. Then the pre-fired billet is transferred into a high-temperature kiln, and the temperature is raised at a heating rate of 3-10°C / min. At ~1650°C, keep warm for 1 to 4 hours each to obtain a lightweight bauxite refractory aggregate with slightly closed pores. The invention has simple process and low cost, and the prepared lightweight bauxite refractory aggregate containing micro-closed pores has the characteristics of low apparent porosity, high closed porosity, small pore diameter and high-temperature medium erosion resistance.

Description

technical field [0001] The invention belongs to the technical field of refractory materials. In particular, it relates to a light-weight alumina refractory aggregate containing micro-closed pores and a preparation method thereof. Background technique [0002] Refractory materials are directly used in high-temperature industrial production processes in various fields of the national economy such as steel, nonferrous metals, cement, glass, ceramics, chemicals, machinery and electric power, and are essential basic materials to ensure the operation and technological development of the above industries. China is currently the world's second largest energy producer and consumer. The "12th Five-Year Plan for Energy Conservation and Emission Reduction" clearly states that energy-saving transformation of industrial kilns should be vigorously promoted. The research and development of high-temperature lightweight refractory materials can greatly reduce the energy consumption of indust...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C04B35/10C04B35/66C04B35/64C04B38/00
CPCC04B35/10C04B35/64C04B35/66C04B38/00C04B2235/656C04B2235/661C04B2235/667C04B2235/77C04B38/0054C04B38/0067
Inventor 顾华志罗志安付绿平黄奥张美杰
Owner WUHAN UNIV OF SCI & TECH
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