Detection method for bis(2-ethylhexyl)amine in leather and textiles
A detection method and textile technology, applied in the field of chemical analysis, can solve problems such as product obstruction, achieve high sensitivity and accuracy, and have good application prospects
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[0050] Example 1
[0051] Cut the leather or textile sample to a size of 2mm×2mm×2mm, weigh 1g±0.1g (accurate to 0.1mg) into a 60ml glass reaction flask, add 10ml of methanol, ultrasonically extract at 60°C for 60min±5min, repeat the extraction once , Combine the two extracts and mix them, use a rotary evaporator to concentrate to about 2ml, slowly blow nitrogen to near dryness, dilute to 1ml with methanol, then filter through a 0.45μm microporous membrane, and then perform gas chromatography-mass spectrometry. Use detection.
[0052] Gas chromatography conditions: Chromatographic column: DB-624, length 30m, film thickness 1.4μm, inner diameter 0.25mm; heating program: initial temperature is 120℃, keep for 1min, increase to 250℃ at a rate of 20℃ / min, keep for 3.5min ; Injection port temperature: 250℃; Injection mode: Splitless; Injection volume: 1μL; Carrier gas: Helium, purity ≥99.999%; Flow rate: 1.5ml / min; Quantification by external standard method. Mass spectrometry condition...
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[0053] Example 2
[0054] The detection method is basically the same as in Example 1. The only difference lies in the heating program: the initial temperature is 100°C, keep it for 1 min, increase to 250°C at a rate of 30°C / min, and keep it for 7 min. The chromatographic results are as follows image 3 As shown, it can be seen that diisooctylamine can be separated, but compared with Example 1, the response value is lower, the peak time is earlier, and the analysis time is longer.
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