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A method for sweating and producing insensitive wax for explosives

An insensitive and explosive technology, applied in non-explosive desensitizers/passivators, explosives, non-explosives/non-thermal components, etc., can solve the problem that the oil content index cannot meet the technical index requirements of insensitive wax for explosives, and the It is suitable for the production of insensitive wax products for explosives, but cannot be used to produce insensitive wax products for explosives, etc., to achieve the effects of low operating costs, simple production process, and reduced production costs

Active Publication Date: 2018-12-18
CHINA PETROLEUM & CHEM CORP +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Experiments have shown that when ordinary sweating and deoiling processes produce high melting point paraffin products with a melting point of about 70°C, even if the method of prolonging the sweating time and increasing the sweating termination temperature is adopted, the oil content on the wax in the later stage of sweating has nothing to do with the yield, that is, on the wax The oil content does not decrease with the decrease of the yield, so the ordinary sweat deoiling process is not suitable for the production of insensitive wax products for explosives with a melting point of 70 ℃ ~ 80 ℃, especially the oil content index cannot meet the technical indicators of insensitive wax for explosives Require
[0013] Compared with solvent deoiling, the sweating deoiling process is an intermittent operation, and the product yield is lower and the production cycle is longer, but the sweating deoiling process has the advantages of less investment, simple production process, low operating cost, safe production process, energy saving and It has the advantages of no pollution to the environment, and some manufacturers are still using this method to produce soap wax products
[0014] Over the years, the method of sweating and deoiling has been developed in terms of production equipment and technology, such as CN89214332 (vertical square multi-segment partition sweating tank), CN94223980.6 (dish-type sweating device), CN98233254.8 (paraffin wax sweating tank), CN200920033500.X (new paraffin sweating tank), CN201210508905.0 (a high-efficiency paraffin sweating device), CN201320127680.4 (tubular paraffin deoiling device), etc., have made improvements in sweating and deoiling production equipment; CN91206202 (a High-efficiency paraffin wax sweating tank) has made improvements in the sweating and deoiling process, but these improvements still cannot produce insensitive wax products for explosives with a melting point of 70°C to 80°C

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0043] This embodiment includes: (1) preparation work, (2) cooling - high temperature constant temperature - cooling - low temperature constant temperature crystallization (3) heating - constant temperature sweating, (4) product refining, (5) product blending and other processes.

[0044] (1) Preparation

[0045] Connect the sealing system of the sweating dish (the inner wall is a square of 1m×1m) with the pressurized buffer tank and the compressor; install the decompression buffer tank at the lower part of the sweating dish and connect the vacuum pump; connect the jacket of the sweating dish and the movable coil with the The circulation system is connected, with water as the medium; start the heating function of the circulation system to raise the temperature of the circulation water to 70°C. Put water under the sweating dish plate.

[0046] to 66 # Semi-refined wax (Jinan Petrochemical Company, melting point 66.35°C, oil content 0.76%) is used as raw material, heated and m...

Embodiment 2

[0061] This embodiment includes: (1) preparation work, (2) cooling - high temperature constant temperature - cooling - low temperature constant temperature crystallization (3) heating - constant temperature sweating, (4) product refining, (5) product blending and other processes.

[0062] (1) Preparation

[0063]Prepare a number of stainless steel plates, each stainless steel plate has an external dimension of 0.98 m × 0.98 m × 0.02 m, and drill through holes of φ0.0015 m evenly distributed on the stainless steel plate (the hole is drilled at 0.01m from the edge, and the center of the hole Spacing 0.04m) (the pressure generated by each stainless steel plate is about 1.5kPa), spare.

[0064] Connect the sealing system of the sweating dish (same as Example 1) with the pressurized buffer tank and the compressor; install the decompression buffer tank and connect the vacuum pump at the lower part of the sweating dish; connect the jacket of the sweating dish and the movable coil wit...

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Abstract

The invention discloses a method for sweating and producing deterred wax for explosive. The method is based on common sweating and de-oiling processes, in a sweating process, air-flow passes through a wax layer for carrying liquid state oil in order to compulsively separate wax and oil; at the same time, a solid weight is placed on the wax layer in order to exert pressure intensity to the wax layer for accelerating separating speed of wax and oil and ensuring passing of the air-flow through the wax layer, and the sweating and deoiling solvent-free method can be used for producing deterred wax products for explosive. The method has the advantages of low production equipment investment, simple production process, low operation cost, safety, energy saving without solvent pollution, and the like.

Description

technical field [0001] The invention belongs to the technical field of special wax production, in particular to a method for sweating and producing insensitive wax for explosives. Background technique [0002] Explosives are substances that can burn or decompose quickly. Under the action of certain external energy, they can burn violently (that is, explode) in a very short period of time to generate a large amount of heat and gas, and perform stable detonation work on the outside world. The widespread use of explosives has played an important role in promoting the material civilization of human society. [0003] The main explosive used during the Second World War was TNT, and the commonly used explosives are RDX (RDX, cyclotrimethylammonium trinitrate) and Octogen (HMX, cyclotetramethylenetetranitramine). With the development of science and technology, all kinds of explosives are developing towards high power and high safety. [0004] Under certain conditions, the various ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C10G73/36C06B23/00
CPCC06B23/005C10G73/36
Inventor 张志银孙剑锋郭慧兵赵咏鹤王立言解利辉
Owner CHINA PETROLEUM & CHEM CORP
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