Refrigerator undesirable odor detection method
A detection method and refrigerator technology, applied in the field of odor detection, can solve the problems of large subjective factors, poor reproducibility, inability to judge the specific influence of odor components, and achieve the effect of rapid and accurate separation and analysis
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Embodiment 1
[0070] This embodiment collects and detects and analyzes the gas in the refrigerated and frozen storage compartment of the 1# refrigerator, including the following steps:
[0071] (1) Collect samples: One end of the Tenax TA sampling tube is connected to the sampling pump, and the other end is placed in the refrigerator, refrigerator or freezer to be tested.
[0072] Quickly close the refrigerator door, set the flow rate of the sampling pump to 50mL / min, and the sampling time to 30min.
[0073] (2) Desorption of sample gas: Place the Tenax TA tube of the collected gas in the thermal desorption instrument, and perform secondary thermal desorption according to the conditions set by the thermal desorption instrument. Desorption temperature of primary adsorption tube: 280°C, desorption time of primary desorption: 10min, flow rate of primary desorption is 40ml / min; high temperature of secondary desorption cold trap: 280°C, desorption time of constant temperature cold trap: 40min, s...
Embodiment 2
[0082] This embodiment collects and detects and analyzes the gas in the refrigerated and frozen storage room of 2# refrigerator, the implementation steps are the same as in Example 1, and the gas chromatogram of the corresponding detection results is as follows Image 6 with Figure 7 ; See Table 2 for the equivalent styrene content conversion results.
Embodiment 3
[0084] This embodiment collects and detects and analyzes the gas in the refrigerated and frozen storage rooms of the 3# refrigerator. The implementation steps are the same as in Example 1, and the gas chromatogram of the corresponding detection results is as follows Figure 8 with Figure 9 ; See Table 2 for the equivalent styrene content conversion results.
[0085] Table 2 Gas composition and equivalent styrene content in refrigerators of Examples 1 to 3
[0086]
[0087]
[0088] ND: not detected
[0089] From the analysis of the conversion results shown in Table 2, it can be seen that although the content of isopentane, pentane and cyclopentane in the refrigerator is relatively high in Example 1, due to the large smell threshold, the amount of styrene equivalent converted into However, the content is not high, so its overall impact on the odor in the storage room of the refrigerator is not great.
[0090] In Example 2, compared with Example 1, the content of isope...
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