Colored photosensitive resin composition, color filter and image display device produced using the same
A technology of photosensitive resin and composition, applied in optics, instruments, optical components, etc., can solve problems such as unfavorable brightness and reliability, and achieve high reliability and contrast characteristics, high contrast characteristics, and excellent sensitivity
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[0160] Synthesis example 1
[0161] Add 30 g of methanol to 2 g of Dodecylpyridinium chloride, and slowly drop it into the completely dissolved solution to dissolve 6 g of Phosphotungstic acid hydrate (Aldrich, P4006) in A solution in 25g of water. After dripping, after stirring at 25-50°C for 4 hours, the precipitate was filtered and washed with water. After filtration, it was dried in a vacuum oven at 50°C for 12 hours to obtain 8.5 g of the following chemical formula A-1. (Refer to Eur.J.Inorg.Chem.2014, 21-35 synthesis.)
[0162] [Chemical formula A-1]
[0163]
Example Embodiment
[0164] Synthesis Example 2
[0165] In place of Dodecylpyridinium chloride, Tetrapropylammonium Hydroxide (TCI, product number T0171) was used instead of Dodecylpyridinium chloride, and 7.3 g of Chemical Formula A-2 was obtained by the same method as in Synthesis Example 1.
[0166] [Chemical formula A-2]
[0167]
Example Embodiment
[0168] Synthesis example 3: Synthesis of binder resin (B)
[0169] Put 100g of propylene glycol monomethyl ether acetate and 100g of propylene glycol monomethyl ether into a flask equipped with a stirrer, thermometer, reflux condenser, dropping funnel, and nitrogen introduction tube, and change the atmosphere in the flask from air to nitrogen. , Put 8.2 g of azobisisobutyronitrile, 3.1 g of monomethacrylate (Hitachi Chemical Co., Ltd. FA-513M) with tricyclodecane skeleton, 55.2 g of 2-ethylhexyl acrylate, 4-methyl 5.9 g of styrene, 85.2 g of glycidyl methacrylate, 6.0 g of n-dodecanethiol. Then, the temperature of the reaction liquid was raised to 80°C while stirring, and the reaction was carried out for 4 hours.
[0170] After lowering the temperature of the reaction solution to normal temperature and replacing the atmosphere in the flask from nitrogen to air, 0.2 g of triethylamine, 0.1 g of 4-methoxyphenol, 43.2 g of acrylic acid, and propylene glycol monomethyl were added fro...
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