Efficient stirring method and device of air-entrapment-free zinc-silicon nitride melt
A stirring method and silicon nitride technology, which are applied in chemical instruments and methods, transportation and packaging, chemical/physical processes, etc., can solve the problems of entrainment and low stirring efficiency, and solve the technical problems of entrainment and low stirring efficiency. Effect
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Embodiment approach 1
[0030] Embodiment 1, under the condition that the power of the high-speed electromagnetic stirring device is 20kW, the rotating speed is 900 rpm, a is 0mm, b is 0mm, c is 0mm, and d is 5mm, after stirring stably for 1 minute and 50 seconds, you can get Zinc-silicon nitride melt with no gas entrainment and uniform distribution of silicon nitride particles6.
Embodiment approach 2
[0031] Embodiment 2, under the condition that the power of the high-speed electromagnetic stirring device is 20kW, the rotating speed is 1200 r / min, a is 20mm, b is 20mm, c is 10mm, and d is 10mm, after 2 minutes of stable stirring, no coil can be obtained Zinc-silicon nitride melt with uniform distribution of gas and silicon nitride particles6.
[0032] It can be seen that under the premise of using variable volume graphite crucible to evacuate and isolate the contact between gas and melt, and then under the condition of high power and high speed electromagnetic stirring, the method of the present invention can efficiently prepare gas-free and evenly distributed silicon nitride particles. zinc-silicon nitride melt.
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