Preparation method of germination accelerating agent
A germination agent and ethephon technology, applied in the agricultural field, can solve problems such as lack of soil organic matter, nutritional imbalance of trees, low yield and inferior jujube fruits, etc., and achieve the effect of low cost, low cost and easy availability of raw materials
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Embodiment 1
[0013] Embodiment 1: a kind of preparation method of accelerating germination agent, comprises the following steps:
[0014] 1) Synthesis of ethephon: add bis(2-chloroethyl)-(2-chloroethyl) phosphonate in the reactor, feed hydrogen chloride gas reaction under stirring to synthesize ethephon, wherein the reaction temperature The temperature is 152°C, the reaction time is 13h, the reaction pressure is 0.51MPa, and the stirring speed is 630r / min. The synthesis method of ethephon is simple, low in cost, moderate in production pressure and the product content is as high as 94%, which is suitable for the industrialized production process in my country. At the same time, the pollution problem existing in the old process is solved;
[0015] 2) Preparation of germination agent: 3 parts of ethephon, 1 part of aloe oil, 1 part of alkyl phosphate salt, 0.2 part of aspartic acid and 8 parts of water-soluble chitosan are mixed in the presence of 60 parts of ethanol to form The germination ag...
Embodiment 2
[0016] Embodiment 2: a kind of preparation method of accelerating germination agent, comprises the following steps:
[0017] 1) Synthesis of ethephon: add bis(2-chloroethyl)-(2-chloroethyl) phosphonate in the reactor, feed hydrogen chloride gas reaction under stirring to synthesize ethephon, wherein the reaction temperature The temperature is 158°C, the reaction time is 14h, the reaction pressure is 0.56MPa, and the stirring speed is 640r / min. The synthesis method of ethephon is simple, low in cost, moderate in production pressure and the product content is as high as 94%. It is suitable for the industrialized production process in my country. At the same time, the pollution problem existing in the old process is solved;
[0018] 2) Preparation of germination agent: 5 parts of ethephon, 4 parts of aloe oil, 2 parts of alkyl phosphate salts, 0.3 part of glycine and 10 parts of water-soluble chitosan are mixed in the presence of 80 parts of ethanol to form a germination agent, Th...
Embodiment 3
[0019] Embodiment 3: a kind of preparation method of accelerating germination agent, comprises the following steps:
[0020] 1) Synthesis of ethephon: add bis(2-chloroethyl)-(2-chloroethyl) phosphonate in the reactor, feed hydrogen chloride gas reaction under stirring to synthesize ethephon, wherein the reaction temperature The temperature is 153°C, the reaction time is 13h, the reaction pressure is 0.52MPa, and the stirring speed is 632r / min. The synthesis method of ethephon is simple, low in cost, moderate in production pressure and the product content is as high as 94%. It is suitable for the industrialized production process in my country. At the same time, the pollution problem existing in the old process is solved;
[0021] 2) Preparation of germination agent: 4 parts of ethephon, 2 parts of aloe oil, 2 parts of alkyl phosphate salt, 0.25 part of proline and 9 parts of water-soluble chitosan are mixed in the presence of 63 parts of ethanol to form a germination The prepar...
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