Protection sleeve with radiation protection function and preparation method thereof
A radiation protection and functional technology, applied in protective clothing, textiles, one-component polyolefin rayon, etc., to achieve uniform coating, reduce self-decomposition, and improve thermal conductivity.
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Embodiment 1
[0020] The protective sleeve with radiation protection function, its preparation method comprises the following steps:
[0021]1) Put the polyester fibers into acetone and ethanol for ultrasonic cleaning for 15 minutes, wash with deionized water and then dry; put them in 1.5mol / L NaOH solution, stir magnetically at 55°C for 15 minutes, wash with deionized water and then dry ; Put the quantitative fiber into the solution containing 0.05mol / LSnCl 2 , 0.2mol / L HCl solution, magnetically stirred for 10min, washed with deionized water and dried; prepared 0.03mol / LAgNO 3 solution and 2mol / L ammonia solution according to the mass ratio of silver ammonia solution of 1:3, put the polyester fiber in the silver ammonia solution for 20min magnetic stirring, wash with deionized water and then dry it for later use; 2) First, the activated polyester The fiber is fixed in the silver salt solution, and the reducing solution twice as much as the silver salt solution is slowly dropped in while ...
Embodiment 2
[0023] The preparation method of the protective sleeve with radiation protection function comprises the following steps:
[0024] 1) Fiber pretreatment: Put the polyester fiber in acetone and ethanol for ultrasonic cleaning for 20 minutes, wash with deionized water and then dry; put it in 2.0mol / L NaOH solution, stir magnetically at 60°C for 25 minutes, and then dry it with deionized water Dry after cleaning; put the quantitative fiber into the 2 , 0.5mol / L HCl solution, magnetically stirred for 15min, washed with deionized water and dried; prepared 0.04mol / LAgNO 3 solution and 3mol / L ammonia solution according to the mass ratio of silver ammonia solution of 1:5, the polyester fiber is placed in the silver ammonia solution and magnetically stirred for 30min, washed with deionized water and dried for later use; pretreatment can remove oil stains and Impurities, using silver ammonia solution to activate the surface of the fiber, abandoning the expensive metal palladium, which n...
Embodiment 3
[0032] Protective sleeve with anti-radiation function. The protective sleeve is made of 30% polyurea microcapsule / PP blend spinning and silver-plated polyester fiber, which is cut and sewn. The protective sleeve not only has the function of self-heating, but also can effectively shield High and low frequency radiation with large fluctuations can be applied to special work occasions to protect the body from radiation hazards. At the same time, its self-heating function can keep the body warm. The heat transfer speed and self-heating sensitivity are high, which expands the application of radiation protection fabrics scope.
[0033] The preparation method of the protective sleeve with radiation protection function includes: fiber pretreatment, silver plating, preparation of emulsion, preparation of polyurea microcapsules, and weaving, specifically including the following steps:
[0034] Fiber pretreatment: Put the polyester fiber into acetone and ethanol for ultrasonic cleaning f...
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