Preparation method of composite wallpaper for purifying indoor air
An internal air, clean room technology, applied in textiles, papermaking, fiber processing, etc., can solve the problems of low adsorption rate, fast saturation speed, high material cost, and achieve the effect of improving binding force, improving service life, and improving adsorption
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[0022] The invention provides a kind of preparation method of the composite wallpaper for purifying indoor air, comprising the following steps:
[0023] (1) Preparation of purifying agent
[0024] (1.1) Dissolve tetraisopropyl titanate and tin tetrachloride in absolute ethanol, then add IRMOFs material, ultrasonically disperse, adjust the pH value of the mixed system to 5.0-5.5, and then adjust the mixed system at 110-150 The reaction was sealed at ℃ for 2-3 hours, and the product was centrifuged and washed to obtain the intermediate product A;
[0025] (1.2) After polyepichlorohydrin-dimethylamine is uniformly dispersed in water, intermediate product A is added, then redox graphene is added, ultrasonic treatment is performed for 1-3 hours, and then the precipitate is centrifuged to obtain intermediate product B;
[0026] (1.3) Calcining the intermediate product B at 400-500° C. for 3-5 hours in an inert gas atmosphere to obtain the purifying agent;
[0027] (2) Add 2 to 5 t...
Embodiment 1
[0045] A preparation method for a composite wallpaper for purifying indoor air, comprising the following steps:
[0046] (1) Preparation of purifying agent
[0047] (1.1) Dissolve tetraisopropyl titanate and tin tetrachloride in 2 times the amount of absolute ethanol, then add IRMOFs material, ultrasonically disperse, adjust the pH value of the mixed system to 5.0, and then mix the mixed system at 120 The reaction was sealed at ℃ for 2 hours, and the product was centrifuged and washed to obtain intermediate product A;
[0048] (1.2) After polyepichlorohydrin-dimethylamine is uniformly dispersed in water, intermediate product A is added, then redox graphene is added, ultrasonic treatment is performed for 2 hours, and then the precipitate is centrifuged to obtain intermediate product B;
[0049] (1.3) Calcining the intermediate product B at 450° C. for 4 hours in an inert gas atmosphere to obtain the purifying agent;
[0050] (2) Add 3 times the amount of dimethyl octadecyl pr...
Embodiment 2
[0055] A preparation method for a composite wallpaper for purifying indoor air, comprising the following steps:
[0056] (1) Preparation of purifying agent
[0057] (1.1) Dissolve tetraisopropyl titanate and tin tetrachloride in 2 times the amount of absolute ethanol, then add IRMOFs material, ultrasonically disperse, adjust the pH value of the mixed system to 5.0, and then mix the mixed system at 120 The reaction was sealed at ℃ for 2 hours, and the product was centrifuged and washed to obtain intermediate product A;
[0058] (1.2) After polyepichlorohydrin-dimethylamine is uniformly dispersed in water, intermediate product A is added, then redox graphene is added, ultrasonic treatment is performed for 2 hours, and then the precipitate is centrifuged to obtain intermediate product B;
[0059] (1.3) Calcining the intermediate product B at 450° C. for 4 hours in an inert gas atmosphere to obtain the purifying agent;
[0060] (2) Add 4 times the amount of dimethyl octadecyl pr...
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