Detection method of glucose related substances in acetate compound electrolyte injection
A compound electrolyte and related substance technology, which is applied in the detection field of glucose-related substances in acetate compound electrolyte injection, can solve problems such as unstable retention time of acetate and influence on glucose product detection, and improve product quality and safety Sexuality, the effect of optimizing the process
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Embodiment 1
[0017] A method for detecting glucose-related substances in acetate compound electrolyte injection, comprising the following steps:
[0018] (1) Preparation of system suitability solution: Weigh 24 mg of sodium acetate reference substance, 1 mg of maltotriose reference substance, 1 mg of maltose and isomaltose, 100 mg of glucose reference substance and 2 mg of fructose reference substance, put them in a 10ml measuring bottle, and dilute with water to the mark , shake well, as a system suitability solution.
[0019] (2) Preparation of the test product and self-reference solution: directly take the sample as the test solution, the glucose concentration in the sample is about 10mg / ml; accurately measure 1ml of the test solution, put it in a 50ml volumetric flask, and dilute it with water to the mark , shake well, as control solution A; accurately measure 5ml of control solution A, put it in a 100ml volumetric flask, dilute with water to the mark, shake well, and use it as control...
Embodiment 2
[0023] A method for detecting glucose-related substances in acetate compound electrolyte injection, comprising the following steps:
[0024] (1) Preparation of system suitability solution: Weigh 24 mg of sodium acetate reference substance, 1 mg of maltotriose reference substance, 1 mg of maltose and isomaltose, 100 mg of glucose reference substance and 2 mg of fructose reference substance, put them in a 10ml measuring bottle, and dilute with water to the mark , shake well, as a system suitability solution.
[0025] (2) Preparation of test sample and self reference solution: directly take the sample as the test solution, the glucose concentration in the sample is about 10mg / ml; accurately measure 1ml of the test solution, put it in a 50ml volumetric flask, and dilute with water to the mark , shake well, as control solution A; accurately measure 5ml of control solution A, put it in a 100ml volumetric flask, dilute with water to the mark, shake well, and use it as control solutio...
Embodiment 3
[0029] A method for detecting glucose-related substances in acetate compound electrolyte injection, comprising the following steps:
[0030] (1) Preparation of system suitability solution: Weigh 24 mg of sodium acetate reference substance, 1 mg of maltotriose reference substance, 1 mg of maltose and isomaltose, 100 mg of glucose reference substance and 2 mg of fructose reference substance, put them in a 10ml measuring bottle, and dilute with water to the mark , shake well, as a system suitability solution.
[0031] (2) Preparation of test sample and self reference solution: directly take the sample as the test solution, the glucose concentration in the sample is about 10mg / ml; accurately measure 1ml of the test solution, put it in a 50ml volumetric flask, and dilute with water to the mark , shake well, as control solution A; accurately measure 5ml of control solution A, put it in a 100ml volumetric flask, dilute with water to the mark, shake well, and use it as control solutio...
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