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A kind of dyeing method of natural cationic dye solution and tussah silk

A technology of natural cationic and tussah silk, applied in the field of dyes, can solve the problems of unstable concentration and hue, not bright enough color, unsatisfactory washing and light fastness, etc., to improve the color fastness to washing and rubbing resistance The effect of color fastness

Active Publication Date: 2020-12-15
EASTERN LIAONING UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] Although natural dyes have the advantages of non-toxic, harmless, and pollution-free, natural plant dyes have a complete color spectrum, but the colors are not bright enough, and the washing and light fastness of many varieties are not satisfactory, and their concentration and hue are also unstable.

Method used

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  • A kind of dyeing method of natural cationic dye solution and tussah silk
  • A kind of dyeing method of natural cationic dye solution and tussah silk
  • A kind of dyeing method of natural cationic dye solution and tussah silk

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preparation example Construction

[0036] In the present invention, there is no special limitation on the preparation operation of the natural cationic dye solution, and the technical solution for preparing the dye solution well known to those skilled in the art can be adopted.

[0037] The present invention also provides a method for dyeing tussah silk, which uses the natural cationic dye solution described in the above technical solution to dye, comprising the following steps:

[0038] (1) Immerse tussah silk in natural cationic dye solution at 60-70°C;

[0039] (2) Carry out the first heat preservation of the dye liquor to 80-85°C for 35-45 minutes;

[0040] (3) Carry out the second temperature rise of the dye liquor to 90-95°C, and then carry out the second heat preservation for 25-35 minutes;

[0041] (4) After cooling the dyeing liquor to 45-50° C., dyed tussah silk is obtained.

[0042] In the invention, the tussah silk is immersed in the natural cationic dye solution at 60-70 DEG C. In the present in...

Embodiment 1

[0146] In embodiment 1~3, color depth value test result is respectively as follows Figure 2~4 Shown, the color depth value analysis result in embodiment 1~3 is as follows Figure 5 shown. From Figure 2-5 It can be clearly seen that the K / S value of Example 1, which added bleaching powder and sulfuric acid in the berberine dyeing process, did not change greatly before and after soaping, but in the embodiment of not adding bleaching powder and sulfuric acid in the berberine dyeing process 3 The K / S of tussah silk changed significantly before and after soaping, and the K / S value decreased significantly. According to the above analysis, the addition of bleaching powder and sulfuric acid in the experimental process has a greater impact on the color fastness of tussah silk to washing, which can improve the berberine. The dyeing rate on tussah silk improves the color fastness to rubbing and color fastness to washing.

[0147] In embodiment 4~13, dye uptake rate test result is as...

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Abstract

The invention provides natural positive ion dye liquor and a tussah silk dyeing method. The natural positive ion dye liquor is prepared from the following ingredients in mass content: 0.2 to 1.0% of berberine, 0.01 to 0.02% of bleaching powder, 0.1 to 0.5% of sulfuric acid, 0.3 to 0.6% of leveling agent, 0.8 to 1.2% of sodium acetate and the balance of water. According to the natural positive iondye liquid disclosed by the invention, the berberine is utilized as dyestuff, so that color of the dyed tussah silk is bright; the certain amount of bleaching powder and sulfuric acid are utilized tomodify the berberine, so that the prepared natural positive ion dyestuff can improve washing-resisting color fastness and wear-resisting color fastness. Experimental results show that after the tussahsilk is dyed by the natural positive ion dye liquor disclosed by the invention, the washing-resisting color fastness can reach 4 to 5 levels, and the wear-resisting color fastness can reach 4 to 5 levels.

Description

technical field [0001] The invention relates to the technical field of dyes, in particular to a natural cationic dye solution and a dyeing method for tussah silk. Background technique [0002] For a long time, synthetic dyes such as acid dyes, neutral dyes and reactive dyes have been mainly used in the dyeing of silk fabrics, but it has been found that acid dyes have poor color fastness, especially wet treatment fastness, and neutral dyes have better fastness than acid dyes, but There are few bright colors in the chromatogram. Reactive dyes are the only dyes that combine with silk fibers by covalent bonds. They have good color fastness and bright colors, but it is difficult to peel off and correct when the shades do not match. Synthetic fibers and synthetic dyes have the potential to cause skin diseases in humans. [0003] Natural dyes and natural fibers have the advantages of non-toxic, harmless, and pollution-free. Silk dyed with natural dyes has a natural, elegant, and n...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D06P1/41D06P1/653D06P3/04
CPCD06P1/41D06P1/6533D06P3/041
Inventor 程德红韩玲路艳华林杰王勃翔李佳
Owner EASTERN LIAONING UNIV
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