Photocatalytic film and method for preparing photocatalytic film by vapor deposition method
A photocatalytic film and photocatalyst technology, applied in chemical instruments and methods, physical/chemical process catalysts, chemical/physical processes, etc., can solve problems such as low concentration and difficult enrichment, affecting photocatalytic activity, and narrow visible light response range
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[0088] (3) The preparation method provided by the invention has simple process and strong operability;
[0089] (4) The raw materials of the preparation method provided by the present invention are easy to get, the area of the photocatalytic film produced is controllable, and a composite film with a larger area can be prepared, which is suitable for the treatment of actual continuous sewage;
[0090] (5) The photocatalytic film provided by the present invention can also carry out continuous photocatalytic treatment of flowing wastewater.
Embodiment 1
[0095] Get the carbon paper prepared by the present invention as base film material, and its area is 15cm2 , placed flat in a crucible with a lid;
[0096] Then pave 7.5g of precursor urea on the bottom of the basement membrane material, and the ratio of the quality of the precursor to the area of the basement membrane material is 0.5g / cm 2 ; and the vertical distance between the basement membrane material and the precursor is 1cm;
[0097] Put the above-mentioned crucible containing the base film material and the precursor in a tubular muffle furnace, replace the muffle furnace with nitrogen, turn on the power of the muffle furnace, increase the temperature at a rate of 3.3°C / min to 550°C, and calcine for 3h. A photocatalytic film was obtained, which was recorded as 1.
Embodiment 2
[0099] The method used in this embodiment is the same as that in Example 1, except that the amount of the precursor used is that the ratio of the mass of the precursor to the area of the base film material is 0.3 g / cm 2 . Finally, the photocatalytic film was obtained, denoted as 2.
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