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A kind of preparation method of disperse dark blue dye and application thereof

A technology for dispersing dark blue dyes, which is applied in the field of preparation of disperse dark blue dyes, can solve problems such as unsatisfactory thermal migration fastness and washing fastness, affect various color fastnesses of textile dyeing, environmental pollution, etc., and achieve good washing fastness , Excellent fastness and high strength

Active Publication Date: 2020-05-26
ZHEJIANG BOAO DYESTUFF IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The dark blue monomer dyes currently available on the market are expensive and cannot meet the printing and dyeing needs of such textiles. The market urgently needs a cheap and good-quality substitute, and its thermal migration fastness and washing fastness are not ideal. , affecting the various color fastnesses of textile dyeing, and bringing more pollution to the surrounding environment

Method used

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  • A kind of preparation method of disperse dark blue dye and application thereof
  • A kind of preparation method of disperse dark blue dye and application thereof
  • A kind of preparation method of disperse dark blue dye and application thereof

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Embodiment Construction

[0022] The present invention will be further described in detail below in conjunction with specific embodiments: a preparation method of disperse dark blue dye, comprising the following steps: 1, mixing dye monomers or finished dyes with auxiliary agents, mixing the dye monomers or finished products used The dyestuff comprises the following components: dye monomer A shown in formula (I), dye monomer B shown in formula (II), dye monomer C shown in formula (Ш), dye monomer C shown in formula (IV) The dye monomer D shown and the dye monomer E shown in formula (V) and auxiliary agents;

[0023]

[0024]

[0025] where R 1 = Cl or Br, R 2 =COCH 3 or OCOCH 3 .

[0026]

[0027] where R 1 = Br or Cl, R 2 =CH 2 CH 3 or CH 2 CH 2 CH 3 .

[0028]

[0029] In the formula, R=H or Br.

[0030]

[0031] The auxiliary agent is one of the following or a mixture of two or more in any proportion: naphthalenesulfonate formaldehyde condensate, alkylnaphthalenesulfonate...

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Abstract

Disclosed in the present invention is a dispersed dark blue dye preparation method, comprising the following steps: 1) mixing dye monomers or finished dye with an auxiliary agent, the mixed dye after mixing comprising dye monomer A as shown in formula (I) having a mass fraction of 0.1-70%, dye monomer C as shown in formula (III) having a mass fraction of 0.1-15%, and the remaining mass being the auxiliary agent; in formula (I), R=CH3 or CH2CH3; and in formula (III), R1=CL or Br and R2=COCH3 or OCOCH3; 2) adding an appropriate amount of water to grind until the dispersion is uniform; and 3) spray-drying. The dye prepared using the present method has the advantages of a high dyeing rate, good washing fastness, excellent fastness, low thermal migration resistance, high strength, and relatively low price.

Description

technical field [0001] The invention belongs to the technical field of disperse dyes, in particular to a preparation method and application of disperse dark blue dyes. Background technique [0002] In the quality inspection of textile color fastness, color fastness to washing is an important inspection item, and its test results are directly related to the overall color fastness of the fabric. Some dyes with poor color fastness can also cause varying degrees of damage to the human body and pollute the environment. Therefore, different organizations and countries have formulated corresponding standards to strictly limit the color fastness grades of clothing and home textiles. [0003] Judging from the current situation of textile fabrics, the proportion of fabrics made of a variety of fibers is increasing year by year, such as some domestic high-end fabrics, including polyester blended fabrics. The dark blue monomer dyes currently available on the market are expensive and ca...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09B67/22C09B67/36C09B67/38D06P1/16D06P3/36
CPCD06P1/16D06P3/36
Inventor 吴礼富
Owner ZHEJIANG BOAO DYESTUFF IND