A kind of preparation method of large particle solid incense beads for cigarette tip stick
A technology of large particles and tobacco spices, which is applied in the fields of tobacco, cigarettes, smoke oil filters, etc. It can solve the problems of bad smell, weak cigarette flavoring effect, and fragrance spillage, etc., achieve stable and long-lasting adsorption, and reduce release rate , regular shape effect
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Embodiment 1
[0051] (1) Soluble in 2% acetic acid solution, add polyvinylpyrrolidone K15, stirred, and then slowly drop the ethanol solution containing apolleon and ethylcellulose, stir for 3 h, filter out of liquid, 2 % Of the acetic acid solution is soaked in 24 h, washed repeatedly to neutral, vacuum dry, to obtain polyvinylpyrrolidone-chitosan-ethylcellulose copolymers, wherein the weight ratio of chitosan, polyvinylpyrrolidone and ethylcellulose is 1.5: 1: 1, the concentration of citracetal in ethanol is 5%;
[0052] (2) The fragrance is added to 1: 1 to 1: 1, and the emulsion is 60 min to obtain an emulsion, wherein the spices are cinnamon and the gumblete extract by weight than 1: 4;
[0053] (3) Polyvinylpyrrolidone-chitosan-ethylcellulose copolymer is dissolved in 2% acetic acid solution, and then the emulsion is slowly added, wherein the polyvinylpyrrolidone-chitosan-ethylcellulose copolymer and emulsification are The weight ratio of the liquid is 1.5: 1, and the additional edge is s...
Embodiment 2
[0056] (1) Soluble in 2% acetic acid solution, add polyvinylpyrrolidone K90, stirred, and then slowly drop the ethanol solution containing apolhanol and ethylcellulose, stir for 4 h, filtrate liquid, 2 The% acetic acid solution is soaked for 30 h, washed repeatedly to neutral, vacuum dried to give polyvinylpyrrolidone-chitosan-ethylcellulose copolymers, wherein the weight ratio of chitosan, polyvinylpyrrolidone and ethylcellulose is 2: 1: 0.5, the concentration of citancetal in ethanol is 10%;
[0057] (2) A 5% Tween 80 aqueous solution was added to 1: 1, and the emulsified solution was added to the emulsion, and the spices were mixed by cinnamonal aldehydrate and gumblete extract by weight than 1: 5;
[0058] (3) Polyvinylpyrrolidone-chitosan-ethylcellulose copolymer is dissolved in 2% acetic acid solution, and then the emulsion is slowly added, wherein the polyvinylpyrrolidone-chitosan-ethylcellulose copolymer and emulsification are The weight ratio of the liquid is 2: 1, and th...
Embodiment 3
[0061] (1) Soluble in 2% acetic acid solution, add polyvinylpyrrolidone K30, stirred and dissolved, then slowly drop the ethanol solution containing apolhanol and ethylcellulose, stir for 4 h, filter out of liquid, 2 The% acetic acid solution is soaked in 28 h, washed repeatedly to neutral, vacuum dried to give polyvinylpyrrolidone-chitosan-ethylcellulose copolymers, wherein the chitosan, polyvinylpyrrolidone and ethylcellulose are the weight ratio of 1.8: 1: 0.7, the concentration of citracetal in ethanol is 6%;
[0062] (2) The fragrance is added to 1: 1 to 1: 1, and the emulsion is 60 min to obtain an emulsion, wherein the spices are cinnamon and the gumblete extract by weight than 1: 4;
[0063] (3) Polyvinylpyrrolidone-chitosan-ethylcellulose copolymer is dissolved in 2% acetic acid solution, and then the emulsion is slowly added, wherein the polyvinylpyrrolidone-chitosan-ethylcellulose copolymer and emulsification are The weight ratio of the liquid is 2: 1, and the mixing ed...
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