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Method for preparing nano-branched copper-silver bimetal/graphene surface-enhanced Raman spectroscopy substrate

A graphene surface, Raman spectroscopy technology, applied in the field of electrochemistry, can solve problems such as limiting the wide application of preparation methods

Inactive Publication Date: 2019-07-23
QINGDAO UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Benefits of technology

This patented technology uses an improved technique for creating surfaces that can detect small molecules called DLB metal complexes on their way through vibrational scatterings during light absorption or reflection processes. By adjusting certain parameters such as wavelength and intensity of incident radiation, this process allows researchers to study how these tiny particles behave differently when exposed to different chemical environments.

Problems solved by technology

This patented technical problem addressed in this patents relates to improving the efficiency at extracting Raman spectra due to improved electronic excitation capabilities and control over the growth process of atomic vibrations during creation processes like deformation of surfaces. Previous techniques were limited in terms of achieving desired results but now offer various advantages: increased sensibility, reduced costs, environmentally friendly nature, and stable long term storage without losing any data stored inside. These advancements make the discovery of effective technologies for producing rare earth sinter powders suitable for applications related to quantum communication devices.

Method used

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  • Method for preparing nano-branched copper-silver bimetal/graphene surface-enhanced Raman spectroscopy substrate
  • Method for preparing nano-branched copper-silver bimetal/graphene surface-enhanced Raman spectroscopy substrate

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Embodiment 1

[0016] (1) Preparation of graphene and graphene paper: graphene oxide was prepared by the modified Hummer method, and then graphene oxide was reduced with vitamin C to prepare graphene. The specific process is briefly described as follows: Take 2 g of graphite, 10 mL of concentrated sulfuric acid and 1 g of P2O5, mix and heat to 80 °C, make it pre-oxidized for 30 min, then cool to room temperature within 6 h, dilute the mixture with distilled water, Suction filtration and washing to neutrality, dry the pre-oxidized graphite and mix it with 50 mL of concentrated sulfuric acid, slowly add 6 g of potassium permanganate, stir, control the temperature below 20 °C, and then place the mixture at 35 °C Stirred in an oil bath for 2 h, then added 280 mL of water to terminate the reaction, and added 5 mL of 30 % H 2 o 2 , the mixture turns bright yellow, and the resulting mixture is dispersed in water, then suction filtered, and the filter cake after suction filtration is washed with 1:...

Embodiment 2

[0019] Example 2. The graphene paper in step (2) in Example 1 was changed to filter paper, and copper-silver bimetal was electrodeposited, and the others were the same as in Example 1. The resulting substrate has only weak Raman enhancement.

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Abstract

The invention provides a method for electrochemically preparing a nano-branched copper-silver bimetal/graphene surface-enhanced Raman spectroscopy substrate, and belongs to the technical field of electrochemistry. The method provided by the invention comprises the following steps of (1) preparing graphene oxide by a redox process using graphite as a raw material, reducing the graphene oxide with vitamin C to obtain graphene, and vacuum-filtering to obtain graphene paper having a thickness of about 10 micrometers; (2) preparing nano-branched copper/silver bimetal by electrodeposition on the graphene paper; and (3) detecting enhancement effect of the nano-branched copper-silver bimetal/graphene by using 4-mercaptobenzoic acid as a detection reagent, wherein the surface enhancement coefficient of the calculated copper silver/graphene (Cu: Ag = 1:1) is 3.7*105 by using 785nm laser. The reason for the high reinforcing effect of the substrate lies in the rough surface of the bimetal, the synergistic effect of copper-silver enhancement, and the chemical enhancement of graphene.

Description

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Claims

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Application Information

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Owner QINGDAO UNIV
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