Method for preparing nano-branched copper-silver bimetal/graphene surface-enhanced Raman spectroscopy substrate
A graphene surface, Raman spectroscopy technology, applied in the field of electrochemistry, can solve problems such as limiting the wide application of preparation methods
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Embodiment 1
[0016] (1) Preparation of graphene and graphene paper: graphene oxide was prepared by the modified Hummer method, and then graphene oxide was reduced with vitamin C to prepare graphene. The specific process is briefly described as follows: Take 2 g of graphite, 10 mL of concentrated sulfuric acid and 1 g of P2O5, mix and heat to 80 °C, make it pre-oxidized for 30 min, then cool to room temperature within 6 h, dilute the mixture with distilled water, Suction filtration and washing to neutrality, dry the pre-oxidized graphite and mix it with 50 mL of concentrated sulfuric acid, slowly add 6 g of potassium permanganate, stir, control the temperature below 20 °C, and then place the mixture at 35 °C Stirred in an oil bath for 2 h, then added 280 mL of water to terminate the reaction, and added 5 mL of 30 % H 2 o 2 , the mixture turns bright yellow, and the resulting mixture is dispersed in water, then suction filtered, and the filter cake after suction filtration is washed with 1:...
Embodiment 2
[0019] Example 2. The graphene paper in step (2) in Example 1 was changed to filter paper, and copper-silver bimetal was electrodeposited, and the others were the same as in Example 1. The resulting substrate has only weak Raman enhancement.
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