Preparation method of radix puerariae tagatose oral liquid

A sugar oral liquid, the technology of Puerarin Tagatose, which is applied in the field of preparation of Gegen Tagatose Oral Liquid, can solve the problems of heavy odor, low puerarin content, bitter taste, etc., to expand the range of application groups, improve drinking taste, and facilitate release Effect

Pending Publication Date: 2021-06-11
林路生物科技(黄石)有限公司
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AI-Extracted Technical Summary

Problems solved by technology

However, the kudzu root solution produced by the soaking method is dark brown, and the puerarin content is low, the taste is bitter, and the smell is very heavy, so it is difficult to directly promote it as a d...
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Method used

Optionally, in one embodiment of the application of the present invention, the step of obtaining the Pueraria Tagatose Oral Liquid after stirring, the step also included is: the Pueraria Tagatose Oral Liquid is sterilized, the temperature of the sterilization The range is 68-70 degrees. By heating and sterilizing the Pueraria Tagatose Oral Liquid at 68-70°C, the bacterial content in the Pueraria Tagatose Oral Liquid can be further reduced, ensuring that the product can be stored for a long time and is convenient for commercial application.
The preparation method of ku...
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Abstract

The invention relates to a radix puerariae tagatose oral liquid preparation method, which comprises: adding 2 parts by mass of radix puerariae powder to 200-500 parts by mass of purified water, and stirring to obtain a first mixture; adjusting the pH value of the first mixture to 6-6.5 by using citric acid, and then adding 0.1-0.4 part of amylolytic enzyme to obtain a second mixture; stirring the second mixture for 6-12 hours, cooling to 48-50 DEG C, and adjusting the pH value of the second mixture to 3-4 with citric acid to obtain a third mixture; adding 0.1-0.4 part of cellulase into the third mixture, stirring for 6-12 hours, and filtering to obtain filtrate; and concentrating the filtrate, adding tagatose, and stirring to obtain the radix puerariae tagatose oral liquid. According to the preparation method of the radix puerariae tagatose oral liquid, release of puerarin is facilitated, and the content of puerarin in the obtained oral liquid is higher than that of puerarin in a radix puerariae solution obtained through a traditional soaking method; the oral liquid contains tagatose, so that the drinking taste can be effectively improved, and the application crowd range of drinks is expanded.

Application Domain

Food science

Technology Topic

MouthfeelStarch hydrolysis +8

Image

  • Preparation method of radix puerariae tagatose oral liquid

Examples

  • Experimental program(1)

Example Embodiment

[0022] In order to facilitate understanding of the present invention, the present invention will be described more fully described with reference to the related drawings. The possible embodiments of the present invention are given in the drawings. However, the present invention can be implemented in many different forms, and is not limited to the embodiments described herein. The embodiments described with reference to the accompanying drawings are exemplary, and the understanding of the disclosure of the present invention is more thoroughly comprehensively comprehensively, and cannot be construed as limiting the invention. Further, the detailed description of the invention is not necessary for the features of the present invention shown, and these techniques may be omitted.
[0023] Those skilled in the relevant art will appreciate that all terms (including technical terms and scientific terms) used herein are the same meaning as generally understood by those of ordinary skill in the art of the present invention. It should also be understood that those terms defined in a general dictionary should be understood as having the meaning unless of the prior art, and unless it is particularly defined as it is, it will not be desirably or too formal. Meaning to explain.
[0024] Those skilled in the art will appreciate that unless specifically declared, the singular forms, "one", "" ",", ", and" "", can include plural form. It should be further understood that the phrase "comprising" in the specification of the present application refers to the features, integers, steps, operations, elements, and / or components, but do not exclude presence or addition of one or more other features. Integer, steps, operations, components, components, and / or groups. It should be understood that the wording "and / or" including one or more associated listed items and all combinations are included.
[0025] The technical solutions of the present invention and how the technical solutions will be described in detail below with specific embodiments.
[0026] The method of preparation of Pueraria Taggosa oral liquid provided by the present invention, such as figure 1 As shown, including the following steps:
[0027] S100: 2 parts of Pueraria powder to 200 to 500 parts of purified water in a mass part, stirring the first mixture. The acquisition of Pueraria usually uses a crushing dry root block, pulverizes the root block into 60-200 megadownload megadownload megadownload megadownload megadownload megadownload. In the subsequent step, the mass parts are also used in the addition of matter or ingredients.
[0028] S200: After the pH of the first mixture was adjusted to 6-6.5, 0.1 to 0.4 parts of starch hydrolase was added to obtain a second mixture. That is, the amount of starch hydrolase is added to 5% to 20% in S100.
[0029] S300: After stirring the second mixture for 6 to 12 hours, it cooled to 48 to 50 ° C, and the pH of the second mixture was adjusted to 3-4 with citric acid to obtain a third mixture. Alternatively, in a specific implementation, the second mixture was stirred for 6 to 12 hours, and the stirring rate was 10-50 revolutions per minute, i.e., at a lower stirring rate, evenly agitated.
[0030] S400: Add 0.1 to 0.4 parts of cellulase to the third mixture, stirred for 6 to 12 hours, filtered. Optionally, in a specific implementation, the step of filtrate the filtrate was filtered after stirring for 6 to 12 hours, filtration apparatus for filtering the diameter of 0.45 microns. Third mixtures can be filtered through a 0.45 microns of precision filtration, and the solid state ingredients in the third mixture can be filtered, so that the solution containing puerarin containing puerarin is effectively separated from other ingredients.
[0031] S500: After concentrating the filtrate, add Taggosa, and gave Pueraria Taggose oral liquid. Optionally, in one of the specific implementations, the filtrate is concentrated in the step of adding Taggosa, the volume of the filtrate is 20% before concentrating, i.e., the concentrated filtrate volume is 5-fifth prior to filtration. I. Greatly increase the content of the puerarin in the unit volume of filtrate, so that the final result of the pueraridal sugar oral liquid has a higher puerarin content. In addition, Taggosa has a sugar of 50-90 sugar to ensure that drinking tastes containing puerarin filtrates are effectively adjusted, which is easy to eat.
[0032] The above step number does not mean that the Puerace Taggosa oral liquid preparation method provided in this application has a strict step limit, only one of the steps of the preparation method of the Pueraria Tagg sugar oral liquid according to the application, for example, it is very likely The above steps S100 to S500 are combined into one step or may be divided into three steps.
[0033] Alternatively, in one embodiment of the present invention, the step of obtaining the puerarch Tag sugar oral liquid after stirring, and the step of being sterilized for the Pueraria Taggose oral liquid, sterilized temperature range 68 -70 degrees. By heat sterilization of Pueraologue Glycemic oral liquid, it is possible to further reduce the bacterial content of the puerarch Taggose oral liquid to ensure that the product can be stored for a long time and facilitate commercial application.
[0034] The puerarial Tagg sugar oral liquid provided by the present invention can add a starch hydrolase and cellulase to a mixture of pueragrar powder, and the pH is adjusted by citric acid, it can make Puerarial plant cell wall loose softening. The release of Puerarin, the guess solution in the oral liquid is higher than the Pueraria solution obtained by the traditional soaking method. It is made into oral liquid with Taggos, which can effectively improve the drinking taste, expand the application population of drinks.
[0035] In combination, in some embodiment, the full process of the preparation of Pueraria Taggosy oral liquid can be:
[0036] Pulk the root block into 60-200 megadownload megadownload megadownload megadownload megadownload megadownload megadownload megadownload megadownload megadownload megadownload megadownload megadownload. The pH of the first mixture was adjusted with citric acid to 6.5, and 0.2 g of starch hydrolyzate was added to the second mixture. The second mixture was stirred at a low speed such that the second mixture was hydrolyzed for 10 hours, and then the temperature of the second mixture after the hydrolysis reaction was cooled to 50 ° C, the pH value of 4 was adjusted to 4 to obtain a third mixture. Weighing 0.1 g of cellulase added to the third mixture, the third mixture was stirred at a temperature of 50 degrees Celsius to allow for 12 hours of reaction. The reaction after the reaction was then filtered through a filtration device having a diameter of 0.45 microns, and the filtrate was obtained. At this time, the filtrate is a pale yellow transparent liquid.
[0037]The volume of the filtrate was concentrated to 1/5 prior to concentration, and the 80-sugar Taggosy syrup was added to the concentrated filtrate, heated to 70 ° C and held for a certain period of time, minimally sterilized, and finally made into Gegen Tag Sugar oral liquid.
[0038] The comparative trial showed that Puerarin was obtained using a normal soaking method, and if soaking the same time used in the preparation method of the Pueraria Tag sugar oral liquid provided by the present application, the puerarin obtained by ordinary soaking method Only about one third of the puerarins provided by this application. The puerarin content provided by the Pueraologue Glycetin Oral Liquidation, the puerarin content is greater than 40 mg per kilogram, which can greatly improve production efficiency and enhance the effective ingredient content in unit products.
[0039] Those skilled in the art will appreciate that the steps, measures, measures, measures, and schemes in the various operations, methods, processes already discussed in this application can be alternate, change, combine, or delete. Further, other steps, measures, measures, schemes, and schemes, and schemes, and schemes, can also be alternate, change, rearrange, decompose, combine or delete. Further, the prior art has the steps, measures, measures, measures, and schemes, and schemes, and schemes, and schemes, and schemes, and the schemes, and the schemes, and decomposition, combination, or deletions can also be alternately, changed, rearranged, decomposed, combined or deleted.
[0040] The term "first", "second" is used only for the purpose of describing, and cannot be understood as an indication or implies a relative importance or implicitting the number of techniques indicated. Thereby, the features of "first", "second" may be defined, and one or more of this feature may be further included. In the description of this application, the meaning of "multiple" is two or more unless otherwise stated.
[0041] It should be understood that although various steps in the flowcharts of the drawings are displayed in accordance with the instructions of the arrow, these steps are not necessarily performed in the order indicated by the arrow. Unless otherwise specified herein, the implementation of these steps does not have a strict order restriction, which can be performed in other orders. Moreover, at least a portion of the steps in the flowcharts of the drawings may include multiple sub-steps or multiple stages, which are not necessarily performed at the same time, but can be performed at different times, and their execution sequence is also It is not necessary to perform in turn, but can be performed or alternately performed with at least a portion of the sub-step or phase of other steps or other steps.
[0042] The above is only the embodiments of the present invention, which should be pointed out that a number of improvements and moisters can also be made without departing from the principles of the present invention, these improvements and moisters are also made without departing from the principles of the present invention. It should be considered as the scope of protection of the present application.

PUM

PropertyMeasurementUnit
Granularity60.0 ~ 200.0mesh

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