Sludge biological asphalt and preparation method thereof
A bio-asphalt and sludge technology, applied in the direction of building structure, construction, building components, etc., can solve the problem of how to use by-products that are not mentioned, and achieve the effect of realizing resource utilization and alleviating dependence
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[0029] The preparation method of the sludge bio-asphalt of the present invention comprises the following steps: a sludge drying step; a sludge reaction step; a solid-liquid separation step; a step of obtaining sludge heavy oil; and a mixing step of sludge heavy oil and petroleum asphalt.
[0030]
[0031] The sludge is dried at 100-110°C, preferably, the sludge is dried at 105-110°C. This is beneficial to the reaction of the sludge in the presence of alcohol and increases the yield of heavy oil from the sludge. The prior art usually directly mixes this sludge with asphalt. In the present invention, it is further processed to improve the performance of sludge bio-asphalt.
[0032]
[0033] Add the dried sludge and alcohol with a weight ratio of 1:10-20 into the reactor, stir and heat, and react for 30-120 minutes at a reaction temperature of 265-300°C and a reaction pressure of 5-11MPa. The temperature was lowered to obtain a reaction mixture. According to one embodiment...
Embodiment 1
[0065] Dry the sludge at 105°C to constant weight;
[0066] Add 40 parts by weight of dried sludge and 600 parts by weight of absolute ethanol into the reactor, seal the device and check the air tightness, then feed nitrogen to replace the air in the reactor, stir and heat, at the reaction temperature The temperature was 275°C, the reaction pressure was 9MPa, and the reaction was carried out for 60 minutes, and the temperature was lowered to obtain the reaction mixture;
[0067] The reaction mixture was suction filtered to obtain solid and mother liquor;
[0068] The mother liquor is distilled under reduced pressure with a rotary evaporator (distillation temperature is 200°C, vacuum degree is 0.1MPa), and concentrated until almost no fraction is separated to obtain sludge heavy oil (black viscous liquid).
Embodiment 2
[0070] The 50# base petroleum asphalt of 95 parts by weight is heated to a flow state at 135° C.;
[0071] Add 5 parts by weight of sludge heavy oil prepared according to Example 1 to the fluid petroleum asphalt, and shear at a high speed at 135°C (shear rate is 2000rpm, and the shear time is 30min) to obtain sludge bio-asphalt .
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