L-shaped powder or blocky organic rock supercritical water oxygen reaction device and use method thereof
A technology of supercritical water and reaction devices, which is applied in the production of bulk chemicals, the preparation of liquid hydrocarbon mixtures, and the petroleum industry. It can solve problems such as explosives, inability to heat in stages, and failure to load organic rock supercritical water-oxygen reaction devices. , to achieve the effect of reducing the risk of explosion and separating efficiently
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Embodiment 1
[0045] When the buried depth of the ore seam is 900m, the heat injection temperature is 400°C, and the pyrolysis sample is block, the specific operation steps of the reaction device of the present invention are as follows:
[0046] 1. Place the lower perforated plate 15 with a hole diameter lower than the sample block size on the clasp 14 of the high-temperature and high-pressure L-shaped reactor 13, and then fill the pre-soaked block sample in the supercritical water-oxygen reaction zone, and fix the high-temperature and high-pressure first method Lan 8, a perforated plate 9 is placed on the end of the axial pressure transmission rod 3, thereby applying a pressure of 23.4 MPa to the block sample;
[0047] 2. Connect the high temperature and high pressure L-shaped reactor 13 with the drainage (salt) system and the oil and gas condensation and collection system, and set the pressure of the first back pressure valve 29, the second back pressure valve 30 and the third back pressur...
Embodiment 2
[0054] When the buried depth of the ore seam is 1200m, the heat injection temperature is 380°C, and the pyrolysis sample is powder, its specific operation steps of the reaction device of the present invention are as follows:
[0055] 1. Place the lower porous plate 15 with a hole diameter lower than the particle size of the powder sample on the clasp 14 of the high-temperature and high-pressure L-shaped reactor 13, and then fill the supercritical water-oxygen reaction zone with pre-soaked powder samples to fix the high-temperature and high-pressure first method Lan 8, a perforated plate 9 is placed on the end of the axial pressure transmission rod 3, thereby applying a pressure of 30 MPa to the powdery sample;
[0056] 2. Connect the high temperature and high pressure L-shaped reactor 13 with the drainage (salt) system and the oil and gas condensation and collection system, and set the pressure of the first back pressure valve 29, the second back pressure valve 30 and the third...
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