Cathode active material of rechargeable lithium battery and rechargeable lithium battery
A negative electrode active material and lithium battery technology, applied in battery electrodes, lithium batteries, active material electrodes, etc., can solve problems such as volume expansion, negative electrode performance deterioration, shrinkage, etc.
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Embodiment 1
[0054] Put the silicon pre-placed in the vacuum chamber at a pressure of 5×10 4 Pa in a helium atmosphere by arc heating to 1700°C to create a silicon atmosphere. The resulting silicon atmosphere is cooled under a helium atmosphere to agglomerate and form ultrafine particles. Ultrafine particles adhere to the inner surface of the vacuum tank. This process was continued for 4 hours to produce silicon ultrafine particles as the negative electrode active material.
[0055] The diameters of the obtained particles were measured using an electron microscope, and were found to be 10nm-200nm in diameter, and they seemed to consist of figure 1 Separated ultrafine particles as shown, such as figure 2 The linearly connected ultrafine particles shown and as image 3 Ultrafine particles agglomerated into agglomerates are shown. The Raman shift measured by Raman spectroscopy is at 500cm -1 A peak and full width at half maximum are shown at 15cm -1 .
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