Pill for expelling wind, eliminating dampness, dredging meridians, activating collaterals, dispelling cold and reliving pain and quality controlling method thereof
A chasing and bone-penetrating technology, applied in pill delivery, bone diseases, measuring devices, etc.
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Embodiment 1
[0099] Weigh 35.38g each of Zhichuan Aconitum, Angelica dahurica, Zhicaowu, Zhifu, Licorice, Ephedra, Chuanxiong, Dilong, Chixiaodou, Chishao, Qianghuo, Asarum, Zhitianxing; , Angelica, Tianma, Fangfeng, Guizhi, Gansong each 17.69g, weigh 7.08g of Myrrha, Poria 70.77g
[0100] [Preparation method] Grind the above twenty-three herbs into fine powder, sieve, and mix well. Add 60g of refined honey and appropriate amount of water, make pellets, and dry. In addition, mix talcum powder, ferric oxide, carmine, and peach gum (ratio 125:7:1:4) as a coating material, coat, and then dry to make every 10 pills weigh 1g to obtain the finished product .
[0101] [Content Determination] Chromatographic conditions of high performance liquid chromatography: use octadecylsilane bonded silica gel as filler, use methanol: water with a volume ratio of 30:70 as the mobile phase, the detection wavelength is 230nm, and the number of theoretical plates Calculated according to the peak of paeoniflor...
Embodiment 2
[0106] Weighing the medicinal materials is the same as in Example 1, and the preparation method is as follows: crush the above twenty-three medicinal materials into fine powder, sieve, and mix well. Add 65g of refined honey and appropriate amount of water, make pellets, and dry. In addition, mix talcum powder, ferric oxide, carmine, and gelatin (ratio 130:5:1:3.5) to make a coating material, coat, and then dry to make every 10 pills weigh 1g to obtain the finished product . The content determination method is the same as that in Example 1, and the measured content of paeoniflorin in the sample is 0.9 mg / g.
Embodiment 3
[0108] Weighing the medicinal materials is the same as in Example 1, and the preparation method is as follows: crush the above twenty-three medicinal materials into fine powder, sieve, and mix well. Add 58g of refined honey and appropriate amount of water, make pellets, and dry. In addition, mix talcum powder, ferric oxide, carmine, and gum arabic (ratio: 128:4:1:5) to make a coating material, coat, and then dry to make every 10 pills weigh 1g, that is, Get the finished product. The content determination method is the same as that in Example 1, and the paeoniflorin content of the sample is measured to be 1.1 mg / g.
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