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Shenbao preparation, its preparing method and quality control method

A preparation and detection method technology, applied in the field of traditional Chinese medicine preparations, can solve problems such as difficult product quality, unstable liquid preparations, and easy precipitation

Active Publication Date: 2011-07-06
ZHEJIANG HUISONG PHARMA
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0025] The main problems in the prior art are: (1) the liquid preparation is unstable, and it is easy to produce precipitation after long-term storage; (2) the production cost is high, and it is inconvenient to carry and transport; (3) the existing dosage forms all contain preservatives; (4) the current All dosage forms have the deficiency of high sugar content, which is not suitable for patients with diabetes and liver disease; (5) the quality control standard of the existing preparations is low, and there are only three physical and chemical identifications in the identification item, the specificity is poor, and there is no content determination, Difficult to really control product quality

Method used

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  • Shenbao preparation, its preparing method and quality control method

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0214] Embodiment 1: the preparation of tablet

[0215] Cnidium 93.3g Chuanxiong 94.3g Cuscuta 220g

[0216] Psoralen 95g Poria cocos 100g Red ginseng 66.7g

[0217] Cumin 48g, Schisandra 120g, Golden Sakura 315.3g

[0218] Atractylodes macrocephala 47.3g Angelica 156g Raspberry 109.7g

[0219] Polygonum multiflorum 248g Plantago seed 55g Rehmannia glutinosa 313.3g

[0220] Lycium barbarum 220g, yam 154.3g, epimedium 315.3g

[0221] Fenugreek 313.3g Astragalus 171.3g Cistanche 157.7g

[0222] Zhi Licorice 47.3g

[0223] The above twenty-two flavors, cnidium, epimedium, angelica, chuanxiong, and cumin are crushed into coarse powder, and 70% ethanol is used as a solvent. After soaking for 48 hours, slowly infiltrate at a speed of 1-3ml per minute, collect The percolation liquid is about 5000ml, ethanol is recovered, concentrated under reduced pressure to a clear paste with a relative density of 1.10 (80°C thermal measurement), filtered, and the filtrate is set aside; the r...

Embodiment 2

[0224] Example 2: Preparation of Chewable Tablets

[0225] Cnidium 140g Chuanxiong 141.5g Cuscuta 330g

[0226] Psoralen 142.5g Poria cocos 150g Red ginseng 100g

[0227] Cumin 72g Schisandra 180g Golden cherry 473g

[0228] Atractylodes 71g Angelica 234g Raspberry 164.5g

[0229] Polygonum multiflorum 372g Plantago seed 82.5g Rehmannia glutinosa 470g

[0230] Lycium barbarum 330g Chinese yam 231.5g Epimedium 473g

[0231] Fenugreek 470g Astragalus 257g Cistanche 236.5g

[0232] Roasted licorice 71g

[0233] The above twenty-two flavors, cnidium, epimedium, angelica, chuanxiong, and cumin are crushed into coarse powder, and 70% ethanol is used as a solvent. After soaking for 48 hours, slowly infiltrate at a speed of 1-3ml per minute, collect The percolation liquid is about 7500ml, ethanol is recovered, concentrated under reduced pressure to a clear paste with a relative density of 1.10 (80°C thermal measurement), filtered, and the filtrate is used for later use; red gins...

Embodiment 3

[0234] Embodiment 3: the preparation of granule

[0235] Cnidium 93.3g Chuanxiong 94.3g Cuscuta 220g

[0236] Psoralen 95g Poria cocos 100g Red ginseng 66.7g

[0237] Cumin 48g, Taste 120g, Golden Sakura 315.3g

[0238] Atractylodes macrocephala 47.3g Angelica 156g Raspberry 109.7g

[0239] Polygonum multiflorum 248g Plantago seed 55g Rehmannia glutinosa 313.3g

[0240] Lycium barbarum 220g, yam 154.3g, epimedium 315.3g

[0241] Fenugreek 313.3g Astragalus 171.3g Cistanche 157.7g

[0242] Zhi Licorice 47.3g

[0243] The above twenty-two flavors, cnidium, epimedium, angelica, chuanxiong, and cumin are crushed into coarse powder, and 70% ethanol is used as a solvent. After soaking for 48 hours, slowly infiltrate at a speed of 1-3ml per minute, collect About 7000ml of the percolating liquid, reclaim ethanol, concentrate under reduced pressure to a clear paste with a relative density of 1.05 (thermal measurement), filter, and the filtrate is for subsequent use; the red ginse...

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Abstract

The present invention relates to a Shenbao preparation, relating to the preparing method and quality control method thereof. It has advantages of good stability, no sugar, no antiseptic, convenient to take and carry, suitable to industrialized production, low production cost, etc, and great marketing potential, and the quality control method can identify Chinese Angelica, Rhizoma Chuanxiong, Common Cnidium Fruit, prepared Tuber Fleeceflower Root, Epimedium Herb, and Malaytea Scurfpea Fruit in the Shenbao preparation, and making content determination on active substance of prepared Tuber Fleeceflower Root-2, 3, 5, 4'-tetrahydroxy diphenylethylene -2-O-b-D- glucoside, active substance of Epimedium Herb-Icariin, active substance of Common Cnidium Fruit-Osthole, and active substance of Chinese Magnoliavine Fruit- Chinese Magnoliavine Fruit methanol.

Description

technical field [0001] The invention relates to a traditional Chinese medicine preparation, in particular to a Shenbao preparation, and to a preparation method and a quality control method of the preparation. Background technique [0002] Impotence, nocturnal emission, low back pain, aversion to cold, frequent urination at night, fatigue, hair loss, tinnitus, leucorrhea in women, menorrhagia and other symptoms caused by kidney deficiency are common and frequently-occurring diseases in clinical practice. The prescription is rigorous, with comprehensive compatibility. It has the functions of reconciling yin and yang, warming yang and tonifying the kidney, calming the nerves and strengthening the essence, and strengthening the body. Because the prescription is supplemented with the product of nourishing yin and regulating qi, it is nourishing but not greasy, warm but not dry. It is a good medicine for tonic in four seasons . Clinically, it can be widely used for the above-ment...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N30/02G01N30/90G01N33/15A61K36/8945A61K9/00A61K9/28A61K9/16A61K9/48A61P15/08A61P13/12A61P1/14
Inventor 毛晓敏
Owner ZHEJIANG HUISONG PHARMA