Collagen short stick using for dacryosolen embolism
A technology of collagen, short rods, applied in the field of medical biomaterials
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Embodiment 1
[0015] 20 grams of commercially available type I collagen, add 0.05% acetic acid solution to 1800ml, add 2% carboxylated chitosan solution 600ml after homogenization, stir evenly and form a viscous gel, put it in a vacuum box and evacuate for 5min, Put it into the syringe pump, use No. 8 injection head to inject at a uniform speed and draw wire, put the bracket into the ultraviolet cross-linking instrument and irradiate it at 254nm for 50min to obtain a Φ0.4mm collagen rod, cut it into a short rod of about 2mm after taking it out, and seal it in a package Post-irradiation sterilization is sufficient.
Embodiment 2
[0017] 15 grams of commercially available type I collagen, add 2% hydrochloric acid solution to 1000ml, add 330ml of 5% low deacetylation degree chitosan solution after homogenization, stir evenly and form a viscous gel, put it in a vacuum box to vacuum 5min, put it into the manual syringe, select the No. 60 Irradiate at 15kGy to get a Φ0.6mm collagen rod, take it out and cut it into short rods of about 2mm, seal the package and sterilize it by radiation.
Embodiment 3
[0019] 30 grams of commercially available type I collagen, add 0.5% citric acid solution to 3600ml, add 0.8% chitosan hydrochloride solution 1200ml after homogenization, stir evenly and form a viscous gel, put it in a vacuum box to vacuum After 5 minutes, put it into a Φ0.5mm mold and freeze-dry it, then put it into a blast drying oven and dry it at 120°C for 2 hours to obtain a Φ0.3mm collagen rod, cut it into short rods of about 2mm after taking it out, seal it and pack it, and sterilize it by radiation.
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