Method for producing a propellant
a technology of propellant powder and powder, which is applied in the direction of explosive working apparatus, cartridge ammunition, weapons components, etc., can solve the problems of high cost, undesirable side effects, and high temperature-dependent performance of propellant powders
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example 1 (
FM 2032n / 9)
[0150] An amount of 90 kilograms of untreated grain, produced with a matrix of 10.5×(19×0.2) mm, is placed inside the treatment apparatus (treatment drum) at a temperature of 16° C. Added to this are 180 grams graphite (0.2 weight % relative to the propellant powder) and a solution of 1440 milliliters of 80% by volume ethanol (16 ml per kilogram propellant powder) and 225 grams of polytetrahydrofuran 650 (0.25 weight % relative to the propellant powder).
[0151] In the gastight, sealed drum, the mixture is mixed at 16° C. while rotating at 14 rpm for 30 minutes. Following this, the lid is removed from the polishing drum and the solvent is allowed to evaporate during a period of 105 minutes.
[0152] The treated propellant powder is dried at 60° C. over a period of 3 days.
[0153]FIGS. 1a-c contrast the test results for burning a propellant powder in the ballistic bomb. The ratio of the momentary pressure P to the maximum pressure Pmax is plotted on the abscissa while the dyna...
example 2 (
FM 2712n)
[0156] Placed into a large treatment apparatus are 220 kilograms of untreated grain, produced with the aid of a 12.0×(19×0.20) mm matrix, and preheated to 30° C. Added to this are 187 grams (0.085 weight % relative to the propellant powder) of graphite and subsequently a solution of 264 grams polytetrahydrofuran 650 (0.12 weight % relative to propellant powder) and 2040 grams 75% by volume ethanol (10.6 milliliter per kilogram propellant powder). The mixture is mixed in the closed drum for 60 minutes at 30° C. and with a rotational speed of 8.25 rpm. Following this, the lid of the polishing drum is removed, another 187 grams (0.085 weight %) of graphite are added and the solvent is allowed to evaporate from the rotating drum during a period of 30 minutes.
[0157] The propellant powder treated in this way is dried over a period of 3 days at 60° C.
example 3 (
FM 2758n)
[0158] This treatment is realized in exactly the same way as for Example 2.
[0159] To confirm the mechanism of the temperature-independent burning of the propellant powder, powder grains were tested in a quenching bomb at different temperatures. A rupture disc opened the bomb at approximately 700 bar and the burned propellant grains are thrown into a water bath and quenched. The recuperated, partially burned propellant grains were then photographed.
[0160]FIGS. 2a-c show the burned propellant grains, which were fired at −40° C., +21° C. and +50° C. It is clearly noticeable that at low temperatures, other form function characteristics contribute to the burning mechanisms than at high temperatures.
[0161]FIG. 3a, on the other hand, shows the pressure bomb test results for the untreated grain FM2708n. FIGS. 3b and 3c show the test results for the two samples FM 2712n and FM2758n. It is quite obvious that the temperature dependence of the propellant powder burning could be redu...
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Abstract
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