Multilayer film for flexible wrapping
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example 1
[0169]The adhesive composition given in Table 1 is prepared by simple hot mixing of the ingredients at 170° C.
[0170]For this adhesive composition a Brookfield viscosity at 190° C. of 14000 mPa·s and a softening temperature of 117° C. are measured.
[0171]This adhesive composition is used for the manufacture of a composite film comprising 2 layers each constituted by an oriented polypropylene film of thickness 20 μm and bonded together by a layer of said composition of thickness comprised between 3 and 5 μm according to the tests.
[0172]In order to produce this film a laminating machine is used the structure of which corresponds diagrammatically to the device shown in FIG. 1. The 2 films of oriented polypropylene are packaged on a reel of 40 cm standard width. The polypropylene reel to be coated is driven by a motor allowing a speed of movement to be given to the substrate ranging up to 600 m / minute. The coating device 5 comprises a lip nozzle marketed by NORDSON under reference BC 70, ...
examples 2 to 8
[0179]The same experimental protocol is applied with each of the different adhesive compositions the contents of which in constituents are given in Table 1.
[0180]The results of the peel test and of the visual test are also given in Table 1.
TABLE 1Content in %Composition12345678Kraton ® D1113BT39.8039.8039.8039.8039.8039.8039.80Vector ® 411139.80Dercolyte ® S11522.39Escorez ® 540049.7534.8324.8859.7014.93Escorez ® 561513.93Escorez ® 1310 LC37.31Escorez ® 2203 LC49.75Regalite ® R10109.9524.8834.8344.78Sylvatac ® RE129.9545.77Irganox ® 10100.500.500.500.500.500.500.500.50Viscosity at 190° C.14000110009000115003000013000700015000(mPa · s)Softening11711311311314011511170temperature (° C.)Extrusion190170170160195185170165temperature (° C.)Peel test at 23° C.2.01.21.12.22.82.20.90.9(N / 15 mm)Visual test33532255
[0181]Vector® 4111 is an SIS copolymer of linear structure having a diblock content of 0% and a styrene content of 19%.
[0182]Compositions 1 to 4 correspond to multilayer films accordi...
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