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55results about How to "·Excellent thermal stability" patented technology

Preparation method of cubic boron nitride and diamond polycrystal with nanometer structure

The invention relates to a preparation method of a cubic boron nitride and diamond polycrystal with a nanometer structure. The preparation method comprises the steps: with hexagonal boron nitride and diamond mixed powder or cubic boron nitride and diamond mixed powder as the raw material, purifying for removing impurities in the raw material, then, assembling a sintering unit without adding any binder, and directly sintering at high temperature and superhigh pressure to prepare the cubic boron nitride and diamond polycrystal with the nanometer structure, wherein diamond accounts for 10-90% of the mass percentage of the raw material. The cubic boron nitride and diamond polycrystal with the nanometer structure is uniform in phase distribution, cubic boron nitride crystal grains have nanometer sizes, and diamond crystal grains are uniformly distributed in the nano cubic boron nitride crystal grains, thus a nanometer cubic boron nitride and diamond interface which is compact in combination and high in strength is formed at a large area. Therefore, the hardness of the high-performance cubic boron nitride and diamond polycrystal with the nanometer structure is equal to that of a diamond monocrystal, and the thermal stability, hardness and wear resistance of the high-performance cubic boron nitride and diamond polycrystal with the nanometer structure are also remarkably higher than those of a diamond polycrystal containing a metal binder.
Owner:HENAN UNIVERSITY OF TECHNOLOGY

Bacteria cellulose pervaporation membrane and uses thereof

InactiveCN101234299ASolve the problem that the thickness uniformity is difficult to controlAddressing Chemical StabilityDistillationCulture fluidMicrobiology
The invention provides a bacterial cellulose pervaporation membrane, which is characterized in that the preparation method is as follows: Acetobacter xylinum DT4.2 strain of the active wood fermentation is put into the seed culture fluid and shaking cultured at constant temperature of 25 to 32 DEG C for 8 to 24 hours; the seed solution is put into the fermentation culture solution to be evenly shaken; and then the fermentation culture solution is moved to the container for culturing for 7 to 15 days at the constant temperature of 25 to 32 DEG C; pellicle membrane formed on the surface of the fermentation solution is taken out and then is processed by the alkali liquor with the quality concentration of 1 to 20 percent; the residual alkali liquor in the membrane is washed to neutrality by the deionized water to prepare into the membrane after drying. The invention also discloses the application of the membrane. The preparation method of the membrane has the advantages of simple preparation, good mechanical and chemical property, excellent heat stability, strong hydrophilicity, high separation choice to the water in the organic water solution at lower temperature, long service life; moreover, the membrane material itself can be biodegradation which is a environmental friendly material.
Owner:许春元

Low cost environmental protection ultra-tough rigid polyvinyl chloride nano compound capable of injection molding and preparation method

The invention discloses a low cost environmental protection ultra-tough rigid polyvinyl chloride nano compound capable of injection molding and a preparation method. The raw material of the compound comprises the components by weight parts: 100 parts of polyvinyl chloride, 10 to 100 parts of nano calcium carbonate, 4 to 100 parts of acrylonitrile-butadiene-styrene terpolymer, 1 to 3 parts of lanthanum tin compound stabilizer, 1 to 3 parts of acrylate processing aid, 1 to 3 parts of inner lubricant and 0.3 to 1 part of outer lubricant. The low cost environmental protection ultra-tough rigid polyvinyl chloride nano compound capable of injection molding is obtained after mixing and cooling the raw materials in a high-speed mixer and granulating in a conical twin-screw extruder. In the invention, the advantages of good flame retardance, strong rigidity and low price of polyvinyl chloride resin, strong rigidity, toughening property for polyvinyl chloride and low price of the nano calcium carbonate, impact resistance, low temperature resistance, easy molding and processing and the like of ABS (Acrylonitrile Butadiene Styrene) are integrated; the product has low price, environmental protection performance, ultra-high toughness, good comprehensive mechanical property and good processing fluidity, and has wide application prospect and obvious social benefit in the fields of household appliance elements, automobile instruments and the like.
Owner:ZHEJIANG UNIV

Star silsesquioxane-grafted acrylic ester-sulfonated styrene segmented copolymer and preparation method thereof

The invention relates to a star silsesquioxane-grafted acrylic ester-sulfonated styrene segmented copolymer and a preparation method thereof. The star silsesquioxane-grafted acrylic ester-sulfonated styrene segmented copolymer is a star hybrid macromolecule which adopts the silsesquioxane as a core and grafted acrylic ester segmented styrene as an arm. The synthesis method of the star silsesquioxane-grafted acrylic ester-sulfonated styrene segmented copolymer comprises the following steps of: synthesizing star silsesquioxane-grafted acrylic ester-styrene segmented copolymer by adopting silsesquioxane containing active chlorine as an initiator, selecting several types of acrylic ester, styrene and the like as comonomer and adopting cuprous chloride/pentamethyl divinyl triamine as a catalytic system through a two-step atom transfer free radical polymerization method; obtaining star silsesquioxane-grafted acrylic ester-sulfonated styrene segmented copolymer through vitriolization; and obtaining star silsesquioxane-grafted acrylic ester-sulfonated styrene segmented copolymer macromolecules of different structures by controlling the length of each POSS (Polyhedral Oligomeric Silsesquioxane) star arm, i.e., the constitution and the length of each block, so that the performances of the star silsesquioxane-grafted acrylic ester-sulfonated styrene segmented copolymer and the proton exchange membrane thereof are adjusted.
Owner:NORTHWESTERN POLYTECHNICAL UNIV

Preparation method of pore-filing type proton exchange membrane taking double ether crosslinked porous polybenzimidazole imide as base

InactiveCN104629081AExcellent thermal stabilityImprove mechanical strength and poor dimensional stabilitySolid electrolyte fuel cellsFunctional polymersEther
The invention belongs to the technical fields of functional polymer materials and electrochemistry and in particular relates to a preparation method of a pore-filing type proton exchange membrane taking double ether crosslinked porous polybenzimidazole imide as a base. The preparation method of the pore-filing type proton exchange membrane taking the double ether crosslinked porous polybenzimidazole imide as the base comprises the following steps: firstly synthesizing polybenzimidazole imide provided with a cross-linkable imidazole group on a main chain, preparing the synthesized polybenzimidazole imide into a membrane solution, adding a double ether crosslinking agent, reacting with the imidazole group, a crosslinking sulfonated polyimide polymer in a membrane forming process, adding a pore-forming agent at the same time to form a crosslinked porous polybenzimidazole imide membrane, and finally compounding the crosslinked porous polybenzimidazole imide membrane with perfluorosulfonate resin, so that the pore-filling type proton exchange membrane is obtained. A basement membrane gives good mechanical properties to the pore-filling type membrane, and the pore-filling type membrane has high dimensional stability; meanwhile, the proton conductivity of a perfluorosulfonate membrane is not greatly reduced. The preparation method of the pore-filing type proton exchange membrane taking the double ether crosslinked porous polybenzimidazole imide as the base has the advantages that the preparation technology controllability is good; and compared with the traditional perfluorosulfonate membrane, the obtained pore-filling type proton exchange membrane has high mechanical strength and good dimensional stability and has broad application prospect in a polymer electrolyte membrane fuel cell.
Owner:TONGJI UNIV

High-strength carbon fiber shielding paper and preparation method thereof

InactiveCN103726394AImprove shielding effectExcellent chemical stabilitySpecial paperPaper/cardboardFiberCarbon fibers
The invention discloses high-strength carbon fiber shielding paper and a preparation method thereof. The shielding paper comprises carbon fibers, plant fibers and conductive particles, wherein the carbon fibers and the plant fibers are randomly and uniformly distributed in a plane, micron-sized holes are formed among the plurality of fibers to form a three-dimensional reticulated structure, and the conductive particles are existent between the surfaces and the holes of the fibers; the carbon fibers are 1 mm to 20 mm in length; the plant fibers comprise wood fibers, grass plant fibers, bast fibers, seed hair fibers or combination of the wood fibers, the grass plant fibers, the bast fibers and the seed hair fibers; the conductive particles comprise carbon black with the particle size of 1 nm to 100 nm, silver coated copper powder, conductive rubber or combination of the carbon black, the silver coated copper powder and the conductive rubber. The shielding paper has the advantages of uniform porous structure and excellent ventilation property, shielding performance and mechanical strength; in addition, air filter paper can be used to the fields of energy resources, electromagnetic wave shielding, antistatic packaging, adsorption separation, aerospace and the like.
Owner:TAICANG PAIOU TECH CONSULTING SERVICE

Organic silicon flame-retardant pressure-sensitive adhesive tape and preparation method thereof

The invention discloses an organic silicon flame-retardant pressure-sensitive adhesive tape. The organic silicon flame-retardant pressure-sensitive adhesive tape comprises a substrate layer, an adhesive agent layer and a release layer, wherein the substrate is a flame-retardant cotton paper layer; flame-retardant filler is filled with the inner part of the flame-retardant cotton paper layer; the flame-retardant filler is prepared from the following components in parts by weight: 30 parts to 50 parts of modified plant fibers, 8 parts to 10 parts of asbestos powder, 6 parts to 8 parts of flame-retardant fibers, 3 parts to 5 parts of nano-aluminum hydroxide, and 10 parts to 20 parts of vegetable glue. The invention also provides a preparation method of the organic silicon flame-retardant pressure-sensitive adhesive tape. The adhesive tape disclosed by the invention has high tensile strength, high softness performance, high viscosity and high stability while the adhesive tape has high flame retardance property; and compared with conventional halogen, the organic silicon flame-retardant pressure-sensitive adhesive tape is relatively high in flame retardance and is more environmentally friendly.
Owner:SHENZHEN NIKTO TAPE NEW MATERIAL CO LTD

Cobalt (CO) and platinum (PT)-based multilayer thin film having inverted structure and method for manufacturing same

The present invention relates to a cobalt (Co) and platinum (Pt)-based multilayer thin film having a novel structure and perpendicular magnetic anisotropy, and to a fabrication method thereof. More specifically, the invention relates to a cobalt and platinum-based multilayer thin film having perpendicular magnetic anisotropy (PMA), which includes thin cobalt layers and thin platinum layers alternately deposited over a substrate, and has an inverted structure in which a thickness of the thin cobalt layers is greater than that of the thin platinum layers, and to a fabrication method thereof. The cobalt and platinum-based multilayer thin film has a new structure in which the thickness of a magnetic thin layer is greater than that of a non-magnetic thin layer. The multilayer thin film may be easily applied as a free layer and a pinned layer in a magnetic tunnel junction by controlling the perpendicular magnetic anisotropy energy depending on the thickness ratio of the layers. Also, the multilayer thin film has excellent thermal stability, and thus maintains its PMA energy density even after being subjected to a heat treatment process. In addition, it enables a fine amount of in-plane magnetic anisotropy to be formed by heat treatment so as to reduce the critical current density required for magnetization switching. Therefore, it may be advantageously used for high-performance and high-density MRAM.
Owner:SK HYNIX INC

Method for preparing lignin sulfonate by utilizing papermaking black liquid

ActiveCN108314789AHeating evenlyHeat release time shortenedWater insolubleFORMALDEHYDE SOLUTION
The invention discloses a method for preparing lignin sulfonate by utilizing papermaking black liquid. The method comprises the following steps: S1, preparing raw materials: preparing the raw materials such as the papermaking black liquid, anhydrous sodium sulfite and formaldehyde, wherein the use amount of the sodium sulfite is 2.9 to 3.2 mmol per gram of lignin, the use amount of the formaldehyde is 0.8 to 1.2 mmol per gram of lignin, and the formaldehyde is prepared into a formaldehyde solution; S2, performing reaction: adding the papermaking black liquid into a reaction kettle, adding thesodium sulfite and the formaldehyde solution, stirring and heating, gradually heating to 158 to 165 DEG C, and continuously stirring to perform reaction for 2.5 to 3.5 hours, wherein the consumed timein the heating process is 80 to 100 minutes and the temperature is increased by 1 to 5 DEG C per minute; and S3, discharging: cooling after the reaction, and discharging when the temperature is reduced to 60 to 70 DEG C. The lignin sulfonate prepared by the method has high sulfonation degree and excellent tainting property, dispersibility and heat-resistant stability, has low water content and low content of sulfate, calcium, magnesium, iron, water insoluble matters and total reducing matters, has excellent comprehensive quality and can be widely applied in various fields.
Owner:HAINAN JINHAI PULP & PAPER
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