Ethoxy chinoline production method
A technology of ethoxyquin and production method, applied in directions such as organic chemistry, can solve the problems of reducing production efficiency, affecting the quality of ethoxyquin, high toxicity and the like, and achieving the effect of improving production efficiency
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[0014] In a 2 cubic meter reactor, add 1,000 kg of p-aminophenetole, 200 kg of recovered p-aminophenetole, 100 kg of toluene and 125 kg of p-toluenesulfonic acid, start stirring and heat up to 140°C, then start to pass through the rotor The flowmeter drips acetone, and the flow of acetone dripping is divided into four stages:
[0015] The first stage is 70 kg / hour for 6 hours
[0016] The second stage is 50 kg / hour for 6 hours
[0017] The third stage is 30 kg / hour for 10 hours
[0018] The fourth stage is 12 kg / hour for 10 hours
[0019] The whole reaction process takes 32 hours, the reaction temperature is controlled at 140°C to 160°C, the total amount of acetone used is 1140 kg, and the water generated during the reaction is continuously discharged from the water separator. After 24 hours of reaction, replace the water separator The toluene in the tank continued to add dropwise acetone to react for 8 hours. When the reaction reached 32 hours, the reaction solution was ta...
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