Side wall passivation method of reaction ion deep etching processing micro structure
A technology of reactive ions and microstructures, applied in nanostructure manufacturing, nanotechnology, nanotechnology, etc., can solve the problem that the sidewall of the etched pattern is not steep, and achieve the effect of low cost
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Embodiment 1
[0022] (1) Sputter a seed layer of 15nmCr and 85nmCu on the surface of the cleaned plexiglass sample, and then paste the plexiglass sheet on the glass substrate. After the glue is cured, use a microtome to mill the plexiglass. cutting, thinning the plexiglass to a set thickness, and then sputtering a seed layer of 15nmCr and 85nmCu on the upper surface of the plexiglass.
[0023] (2) Spin the glue on the surface of the plexiglass at a speed of 4000r / min, spin the glue for 30 seconds, and the thickness of the glue is 2 μm, then expose to ultraviolet rays for 20 seconds, and develop for 40 seconds to harden the film.
[0024] (3) Then carry out nickel mask electroplating (PH value 4.5, electric current 20mA / cm 2 , the plating time is about 10 minutes), the mask thickness is 2 μm, and the glue is removed with 3% KOH solution, and the Cr / Cu is selectively etched to form a patterned Ni mask.
[0025] (4) Optimizing the etching process: specifically select O 2 and CHF 3 The mixed g...
Embodiment 2
[0029] (1) Sputter a seed layer of 15nmCr and 85nmCu on the surface of the cleaned plexiglass sample, and then paste the plexiglass sheet on the glass substrate. After the glue is cured, use a microtome to mill the plexiglass. cutting, thinning the plexiglass to a set thickness, and then sputtering a seed layer of 15nmCr and 85nmCu on the upper surface of the plexiglass.
[0030] (2) Spin the glue on the surface of the plexiglass at a speed of 4000r / min, spin the glue for 30 seconds, and the thickness of the glue is 2.5μm, then expose to ultraviolet rays for 22 seconds, and develop for 45 seconds to harden the film.
[0031] (3) Then carry out nickel mask electroplating (PH value 4.5, electric current 20mA / cm 2 , the plating time is about 10 minutes), the mask thickness is 2.3 μm, and the glue is removed with 3% KOH solution, and the Cr / Cu is selectively etched to form a patterned Ni mask.
[0032] (4) Optimizing the etching process: specifically select O 2 and CHF 3 The mi...
Embodiment 3
[0036] (1) Sputter a seed layer of 15nmCr and 85nmCu on the surface of the cleaned plexiglass sample, and then paste the plexiglass sheet on the glass substrate. After the glue is cured, use a microtome to mill the plexiglass. Cutting, thinning the plexiglass to a set thickness, and then sputtering a seed layer of 15nmCr and 85nmCu on the upper surface of the plexiglass;
[0037] (2) Spin the glue on the surface of the plexiglass at a speed of 4000r / min, spin the glue for 30 seconds, and the thickness of the glue is 2-3μm, then expose to ultraviolet light for 30 seconds, and develop for 50 seconds to harden the film.
[0038] (3) Then carry out nickel mask electroplating (PH value 4.5, electric current 20mA / cm 2 , the plating time is about 10 minutes), the mask thickness is 3 μm, the glue is removed with 3% KOH solution, and the Cr / Cu is selectively etched to form a patterned Ni mask.
[0039] (4) Optimizing the etching process: specifically select O 2 and CHF 3 The mixed g...
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