Azo dye, colored composition, heat-sensitive transfer recording ink sheet, heat-sensitive transfer recording method, color toner, inkjet ink and color filter
A technology of azo dyes and thermal transfer printing, which is applied in the direction of azo dyes, monoazo dyes, optical filters, etc., and can solve problems such as difficult to obtain optical properties
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[0190] Synthesis Example
[0191]
[0192] Intermediate (7a) Example compound (7)
[0193]
[0194] 4.93 g (0.03 mol) of 3-amino-5-tert-butyl-2H-pyrazole-4-carbonitrile were dissolved in a mixture of acetic acid (6 ml), propionic acid (10 ml) and concentrated hydrochloric acid (10 ml), and It was cooled to 0 °C. To this solution, 2.07 g (0.03 mol) of sodium nitrite was added dropwise at an internal temperature of 5°C or lower. Then stir for 15 min at an internal temperature of 0-5°C. Overlapping solutions are thus prepared. Separately, 5.34 g (0.03 mol) of 6-tert-butyl-3-methyl-1H-pyrazole[5.1-c][1.2.4]triazole were dispersed in 90 ml of acetonitrile, which was then cooled to an internal temperature of 5°C. Into the obtained dispersion liquid, the previously prepared overlapping solution was added dropwise at an internal temperature of 5°C or lower. Then it was stirred at 5° C. for 1 h and at room temperature for 30 min, and 100 ml of water was added dropwise theret...
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