Method to reduce gas-phase reactions in a pecvd process with silicon and organic precursors to deposit defect-free initial layers
A technology of organosilicon compound and organosilicate, which is applied in metal material coating process, coating, gaseous chemical plating, etc.
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[0052] The porogen-containing organosilicate dielectric layer may be deposited on the substrate according to the embodiments described above with respect to FIG. 1 . Films can use PRODUCE® available from Applied Materials, Inc. of Santa Clara, California. The PECVD chamber (ie, CVD chamber) on the system performs the deposition. During deposition, the chamber pressure was maintained at a pressure of approximately 4.5 Torr and the substrate was maintained at a temperature of approximately 350°C. The substrate is set 300mil away from the gas distribution showerhead.
[0053] The substrate is placed on a substrate holder provided within the process chamber. A process gas mixture with an initial gas composition of 1000 seem helium and 700 seem oxygen for the interface layer was introduced into the chamber and the flow rate was stabilized before RF power was initiated. Subsequently, about 500 W of RF power was applied to the showerhead to form a plasma comprising an interfacia...
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