Fluoelectrolysis reactor and reaction method

An electrolysis reaction and reactor technology, applied in the electrolysis process, electrolysis components, cells, etc., can solve problems such as affecting production safety, corrosive liquid leakage, etc., and achieve a stable electrolysis reaction environment, improve productivity, and expand the scope of use. Effect

Active Publication Date: 2008-05-28
叶元珠
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  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the pressure generated in the reaction system by this production method can easily lead to the leakage of corrosive liquids and affect the safety of production.

Method used

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  • Fluoelectrolysis reactor and reaction method
  • Fluoelectrolysis reactor and reaction method
  • Fluoelectrolysis reactor and reaction method

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Embodiment Construction

[0030] Preferred embodiments of the present invention are described in detail below.

[0031] As shown in Figure 1, the present invention provides a reactor 100 for fluorination electrolysis, which includes an electrolysis reactor 105, on which a kettle cover 103 is provided for sealing the reactor 105, and a sealing device 111 can also be provided To ensure the dynamic sealing state of the reactor, for enhancing the degree of safety; the reactor 100 also includes at least one pair of electrode plates 108, a pair of positive and negative electrode leads; and, the electrolysis reactor 105 is also provided with a cooling jacket 106, used For cooling the reactor, the cooling jacket 106 can adopt a liquid cooling method, specifically, the inflow and outflow of cooling liquid or circulating cooling can be realized through the input pipe 104 and the output pipe 110 .

[0032] The reactor also includes at least one pair of cathode and anode positioning screws 107, an upper splint 301...

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PUM

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Abstract

The invention discloses a fluorinated and electrolytic reactor and a reaction method. The reactor includes an electrolytic reaction still, electropads, negative and positive electrode outlet terminals, negative and positive electrode fitted rods, an upper clip, a lower clip, a rotation shaft, a generator and a flow guide ring. Every electropad of similar shape is superposed according to presupposition distance, the middle portion is equipped with at least a first-deflector hole and every first-deflector hole forms into a first-diversion trench. Every electropad is provided with a pair of negative and positive fitted holes which are inserted by the negative and positive fitted rods to fix the electropads and are fixedly connected with every clip. The rotation shaft is fixedly connected with the upper clip, and the generator is connected with the rotation shaft. The electrolytic solution between the electropads can flow orderly by rotating the electropads. The invention has the advantages of simple contracture, convenient assembling and disassembling and high volume rate. The product of the reactor is easy to be controlled and be outlet, which enables the reaction product to better collected and be discharged, improves the productivity of the product, and enlarges the variety of the fluorinated product of electrolytic reaction and the range of use of the electrolysis trench. Besides, the invention also solves the problem that the fluorinated electrolysis trench is difficult to be made bigger.

Description

technical field [0001] The invention relates to an electrolytic reactor for organic electrochemical synthesis, in particular to a rotating electrode plate type fluorination electrolytic reactor and a reaction method. Background technique [0002] In the organic fluorination electrolysis equipment in the prior art, the electrolytic electrodes are all anode plates and cathode plates in a rectangular shape with intervals for cross-insulation, vertically stacked and statically suspended in the electrolytic cell, and connected to the outside of the electrolytic cell by terminal posts. According to the connection mode of the electrodes, it can be generally divided into two types of electrolyzers: monopolar and bipolar. [0003] The electrodes of the same polarity in the unipolar electrolytic cell are connected in parallel with the DC power supply, and the polarity of both sides of the electrodes is the same, that is, both are anodes or cathodes at the same time. The electrodes at...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C25B9/12
Inventor 叶元珠
Owner 叶元珠
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