Rhizoma anemarrhenae extrac
An anemarrhena extract and extract technology, applied in the field of diabetes drugs, can solve the problems of reducing blood sugar, insulin resistance, and serum insulin levels in KK-Ay mice, so as to reduce insulin resistance, improve sensitivity, and greatly The effect of medicinal value and economic benefit
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Embodiment 1
[0022] Example 1 Preparation of Anemarrhena Jiangtang Tablets
[0023] (1) Pulverize the Anemarrhena medicinal material, extract twice with 8 times the volume of 80% ethanol for 1 hour each time, let cool and then filter, combine the filtrates, and concentrate to obtain a thick paste 1.
[0024] (2) Take thick ointment 1, dissolve it with 8 times the volume of water, put it on a macroporous resin column, elute with 5 column volumes of distilled water, and discard the eluent. Elute with 50% ethanol solution for 8 column volumes, concentrate the eluent to no alcohol, let stand, precipitate precipitate, filter, dry and pulverize the precipitate to obtain Extract 1, namely Anemarrhena extract.
[0025] (3) Weigh 250 g of the above Anemarrhena extract, add 250 g of calcium sulfate, and 10 g of crospovidone and mix well. Use an appropriate amount of 80% ethanol as a wetting agent to make a soft material, granulate with a 14-mesh sieve, dry at 60°C and pass through a 12-mesh sieve f...
Embodiment 2
[0026] Example 2 Preparation of Anemarrhena Jiangtang Tablets
[0027] (1) Pulverize the anemarrhena medicinal material, extract twice with 8 times the volume of 80% ethanol, each time for 1 hour, let cool and filter, combine the filtrate, concentrate to obtain a thick paste 1; add 8 times the volume of water to extract the residue after filtration 2 times, 1 each time, filtered while hot, combined the filtrates, and concentrated to obtain a thick paste 2.
[0028] (2) Take thick ointment 1, dissolve it with 8 times the volume of water, put it on a macroporous resin column, elute with 5 column volumes of distilled water, and discard the eluent. 8 column volumes were eluted with 50% ethanol, and the eluate was concentrated to no alcohol, left to stand, precipitated, filtered, dried and pulverized to obtain extract 1.
[0029] (3) Take the thick ointment 2, add 20 times the volume of water to dissolve it, filter it with an ultrafiltration membrane device and an ultrafiltration ...
Embodiment 3
[0032] Example 3 Preparation of Zhimu Jiangtang Capsules
[0033] (1) Pulverize the anemarrhena medicinal material, extract twice with 10 times the volume of 80% ethanol, each time for 1 hour, filter after cooling, combine the filtrate, concentrate to obtain a thick paste 1; add 10 times the volume of water to extract the residue after filtration 2 times, 1 each time, filtered while hot, combined the filtrates, and concentrated to obtain a thick paste 2.
[0034] (2) Take the thick paste 1, dissolve it completely with 8 times the volume of water, and put it on the treated macroporous resin column. Elute with 3 column volumes of distilled water and discard the eluate. The 6 column volumes were eluted with 60% ethanol, and the eluate was concentrated to no alcohol, left to stand, precipitated, filtered, dried and pulverized to obtain extract 1.
[0035] (3) Take the thick ointment 2, add 10 times the volume of water to dissolve it, filter it with an ultrafiltration membrane de...
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