Preparation method of silver solder paste and silver solder paste product
A silver brazing and finished product technology, applied in welding equipment, welding medium, manufacturing tools, etc., can solve problems such as insufficient high temperature life, insufficient wettability of solder, insufficient activity retention time, etc.
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Embodiment 1
[0083] (1) Preparation and pretreatment of raw materials
[0084] Take 33 parts of boric acid, 28 parts of potassium fluoroborate, 25 parts of potassium fluoride, and 2.5 parts of monomeric boron. After removing the impurities in each raw material and drying them, they are respectively ground into 80-mesh uniform powder; then weigh 11.5 parts of distilled water set aside;
[0085] (2) stirring
[0086] Put the raw material weighed in the step (1) into the blender except distilled water, stir for 15 minutes, make the raw material mix evenly, the stirring speed of the blender is 85 rev / min;
[0087] (3) Baking
[0088] Spread the evenly stirred mixture on a baking tray with a thickness of 2 cm, put it in the oven, set the baking temperature to 350°C for 3 hours;
[0089] (4) Grinding
[0090] Take out the lumpy mixture after baking, let it stand for 3 hours, let it cool down to room temperature naturally, put the cooled lumpy mixture into a pulverizer and pulverize it; add 1...
Embodiment 2
[0092] (1) Preparation and pretreatment of raw materials
[0093] Take 40 parts of boric acid, 28 parts of potassium fluoroborate, 20 parts of potassium fluoride, and 2 parts of monomeric boron. After removing the impurities in each raw material and drying them, they are respectively ground into 90-mesh uniform powder; then weigh 10 parts of distilled water. set aside;
[0094] (2) stirring
[0095] Put the raw material weighed in the step (1) into the blender except distilled water, stir for 20 minutes, make the raw material mix evenly, the stirring speed of the blender is 100 rev / min;
[0096] (3) Baking
[0097] Spread the evenly stirred mixture on a baking tray with a thickness of 4 cm, put it in the oven, set the baking temperature to 400°C for 3.5 hours;
[0098] (4) Grinding
[0099] Take out the lumpy mixture after baking, let it stand for 3.5 hours, let it cool down to room temperature naturally, put the cooled lumpy mixture into a pulverizer and pulverize it; add...
Embodiment 3
[0103] (1) Preparation and pretreatment of raw materials
[0104] Take 33 parts of boric acid, 28 parts of potassium fluoroborate, 20 parts of potassium fluoride, and 2 parts of monomeric boron. After removing the impurities in each raw material and drying them, they are respectively ground into 100-mesh uniform powder; then weigh 17 parts of distilled water. set aside;
[0105] (2) stirring
[0106] Put the raw material weighed in the step (1) into the blender except distilled water, stir for 25 minutes, make the raw material mix evenly, the stirring speed of the blender is 140 rev / min;
[0107] (3) Baking
[0108] Spread the evenly stirred mixture on a baking tray with a thickness of 6 cm, put it in the oven, set the baking temperature to 450°C for 4 hours;
[0109] (4) Grinding
[0110] Take out the lumpy mixture after baking, let it stand for 4 hours, let it cool down to room temperature naturally, put the cooled lumpy mixture into a pulverizer and pulverize it; add 17...
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