Method for simultaneously preparing zinc phosphate and sodium chloride by chemical fiber waste residue mud

A technology of zinc phosphate and sodium chloride, applied to chemical instruments and methods, alkali metal chlorides, phosphorus compounds, etc., can solve the problems of wasting transportation costs, unfavorable environmental protection, waste of waste residue and mud elements, etc., to achieve low cost, eliminate Effects of chemical pollution, production process and simple equipment

Inactive Publication Date: 2012-01-11
冯若愚
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Problems solved by technology

[0006] The traditional method of treating waste sludge is usually to filter it into a cake and transport it away for accumulation, which is not conducive to environmental protection and wastes transportation costs, especially the valuable material elements contained in the waste sludge; currently, there is no use of chemical fiber waste sludge to prepare phosphoric acid. Related reports on the method of co-producing sodium chloride with zinc

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  • Method for simultaneously preparing zinc phosphate and sodium chloride by chemical fiber waste residue mud
  • Method for simultaneously preparing zinc phosphate and sodium chloride by chemical fiber waste residue mud

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[0031] specific implementation

[0032] A method for preparing zinc phosphate co-production sodium chloride with chemical fiber waste sludge, comprising the following preparation steps:

[0033] Step A. Send 1000kg of chemical fiber waste sludge to the washing tank 1, first wash the chemical fiber waste sludge with clean water, adjust it into a thin emulsion of chemical fiber waste sludge with a solid content of 40%, and then send it to the first corrosion-resistant reactor 2 Among them, the chemical fiber waste sludge contains 384kg of zinc hydroxide and 36kg of sulfide;

[0034] Step B, drop into hydrochloric acid solution (volume percentage concentration is 26%) in the first anti-corrosion reactor 2 to react, the reaction generates the mixed solution I of zinc chloride and sulfuric acid, and carbon dioxide and hydrogen sulfide gas, the first anti-corrosion reactor The mass ratio of the chemical fiber waste sludge thin emulsion to the hydrochloric acid solution in the cor...

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Abstract

The invention belongs to the technical field of chemical industry three-waste treatment and utilization, and in particular relates to a method for simultaneously preparing zinc phosphate and sodium chloride by chemical fiber waste residue mud. The main technical scheme comprises washing chemical fiber waste residue mud, preparing into diluted emulsion, reacting with hydrochloric acid, and recycling the gas generated during reaction through absorption; adding a small amount of calcium chloride and zinc hydroxide sequentially in the mixed liquid generated after reaction, and filtering after reaction; then carrying out reaction on filtrate and sodium phosphate to produce the mixed solution of zinc phosphate and sodium chloride, and filtering; washing filter cake, drying, crushing, checking weight, and packaging to obtain zinc phosphate powder product; and distilling the sodium chloride solution, cooling and crystallizing, crushing and packaging to obtain the sodium chloride crystal product. According to the method provided by the invention, not only is waste mud generated by the chemical fiber production industry treated effectively, the chemical industry pollution is eliminated, but also the chemical fiber waste mud can be changed into zinc phosphate and sodium chloride products with economic value, the production process and the device thereof are simple, and the cost is low.

Description

technical field [0001] The invention belongs to the technical field of treatment and utilization of three chemical wastes, in particular to a method for preparing zinc phosphate and co-producing sodium chloride with chemical fiber waste residue. technical background [0002] Fiber is a necessity for social production and life, and a basic material for the textile industry. The type and quantity of fibers and the quality are important symbols of a country's production, technology and living standards. In today's society, the types of fibers can be summarized into three categories: plant fiber, dynamic fiber and chemical fiber; chemical fiber is the product of the development of modern industry; chemical fiber is made of natural polymer compounds or artificially synthesized polymer compounds. Fibers with textile properties produced by silk stock solution, spinning and post-processing processes; in 1985, the world's chemical fiber output was more than 1 million tons, accountin...

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C01B25/37C01D3/04
Inventor 王嘉兴
Owner 冯若愚
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