Prodrugs
A prodrug-free technology, applied in drug combinations, antineoplastic drugs, pharmaceutical formulations, etc., can solve problems such as slow release and prodrugs that cannot induce tumor remission
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[0046] HPLC system
[0047] Method A: Unless otherwise indicated, use a solvent delivery system (HPLC pump 422), variable wavelength UV-VIS detector (HPLC detector 430), and Nucleosil Reverse phase HPLC analysis of all compounds was performed on a Kontron system on a C-18 column (100-5, 250 x 4 mm, Macherey-Nagel). For peak integration, Geminyx software (v1.91 from Goebel Instrumentelle Analytik, FRG) was used. HPLC conditions: flow rate: 1 mL / min, gradient: 0-5 min 100% mobile phase A; 5-35 min increase to 100% mobile phase B; 35-40 min 100% mobile phase B; 40-45 min decrease to 100 % Mobile Phase A; 45-50 minutes 100% Mobile Phase A; Mobile Phase A: 30% CH 3 CN, 70% water + 0.1% TFA, mobile phase B: 70% CH 3 CN, 30% water + 0.1% TFA, injection volume: 50 μL.
[0048] Method B: Using with a Merck F-1050 spectrofluorophotometer (EX. 490nm, EM. 540nm) and a λ1000 visible detector from Bischoff Attached BioLogic Duo-Flow System from Biorad (Munich, Germany) for HPLC to st...
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